9-(4’-([2,2’:6’,2’’-terpyridin]-4’-yl)[1,1’-biphenyl]-4-yl)-9H-carbazole

Base Information

Chemical Name:9-(4’-([2,2’:6’,2’’-terpyridin]-4’-yl)[1,1’-biphenyl]-4-yl)-9H-carbazole
CAS No.:1393350-33-8
Molecular Formula:C₃₉H₂₆N₄
Molecular Weight:550.662
Hs Code.:

Synonyms:9-(4’-([2,2’:6’,2’’-terpyridin]-4’-yl)[1,1’-biphenyl]-4-yl)-9H-carbazole

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Chemical Property of 9-(4’-([2,2’:6’,2’’-terpyridin]-4’-yl)[1,1’-biphenyl]-4-yl)-9H-carbazole

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Technology Process of 9-(4’-([2,2’:6’,2’’-terpyridin]-4’-yl)[1,1’-biphenyl]-4-yl)-9H-carbazole

There total 2 articles about 9-(4’-([2,2’:6’,2’’-terpyridin]-4’-yl)[1,1’-biphenyl]-4-yl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 785051-54-9
9-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-9H-carbazole

: 89972-76-9
4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine

: 1393350-33-8
9-(4’-([2,2’:6’,2’’-terpyridin]-4’-yl)[1,1’-biphenyl]-4-yl)-9H-carbazole

Guidance literature:: 9-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-9H-carbazole; 4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine; With potassium carbonate; In tetrahydrofuran; ethanol; water; for 0.166667h; Inert atmosphere;

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; water; at 70 ℃; Inert atmosphere;
DOI:10.1002/cplu.201900213

Reference yield:

: 1122-62-9
2-acetylpyridine

: 1122-91-4
4-bromo-benzaldehyde

: 1393350-33-8
9-(4’-([2,2’:6’,2’’-terpyridin]-4’-yl)[1,1’-biphenyl]-4-yl)-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / 0.5 h / 0 °C

1.2: 2 h / 0 °C

1.3: 24 h / 100 °C

2.1: potassium carbonate / ethanol; water; tetrahydrofuran / 0.17 h / Inert atmosphere

2.2: 70 °C / Inert atmosphere

With potassium carbonate; sodium hydroxide; In tetrahydrofuran; ethanol; water; 2.1: |Suzuki Coupling / 2.2: |Suzuki Coupling;
DOI:10.1002/cplu.201900213