C₂₆H₃₄N₂O₄

Base Information

Chemical Name:C₂₆H₃₄N₂O₄
CAS No.:211430-52-3
Molecular Formula:C₂₆H₃₄N₂O₄
Molecular Weight:438.567
Hs Code.:

C<sub>26</sub>H<sub>34</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₆H₃₄N₂O₄

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Chemical Property of C₂₆H₃₄N₂O₄

Chemical Property:

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Technology Process of C₂₆H₃₄N₂O₄

There total 20 articles about C₂₆H₃₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66500-55-8
cyclohexanone-4-carboxylic acid ethyleneacetal

: 211430-52-3
C₂₆H₃₄N₂O₄

Guidance literature:: Multi-step reaction with 17 steps

1.1: diisopropylamine; BuLi / tetrahydrofuran; hexane / 1 h / 20 °C

1.2: 78 percent / tetrahydrofuran; hexane / 2 h / 20 °C

2.1: diphenylphosphoryl azide; triethylamine / benzene / 0.5 h / Heating

2.2: 65 percent / benzene / 5 h / Heating

3.1: 94 percent / osmium tetroxide; N-methylmorpholine N-oxide / acetone; H₂O; 2-methyl-propan-2-ol / 5 h / 20 °C

4.1: 86 percent / 4-(N,N-dimethylamino)pyridine / pyridine / 4 h / 20 °C

5.1: 92 percent / imidazole / dimethylformamide / 4.5 h / 20 °C

6.1: H₂ / 5 percent Pd/C / methanol / 3 h

7.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / benzene / 3.5 h / Heating

8.1: potassium carbonate / acetonitrile / 2.5 h / 20 °C

9.1: 964 mg / tetrabutylammonium fluoride / tetrahydrofuran / 15 h / 20 °C

10.1: 82 percent / diphenylphosphoryl azide; triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 2 h / 20 °C

11.1: 75 percent / H₂ / 5 percent Pd/C / methanol / 1.5 h

12.1: lithium hydroxide / H₂O / 0.67 h / 20 °C

13.1: 234 mg / diphenylphosphoryl azide; triethylamine / dimethylformamide / 1.5 h / 20 °C

14.1: 56 percent / sodium hydride / tetrahydrofuran / 1.5 h / 20 °C

15.1: lithium diisopropylamide / tetrahydrofuran / 0.33 h / -78 °C

15.2: 85 percent / tetrahydrofuran / 0.33 h / -78 °C

16.1: triethylamine / CH₂Cl₂ / 1 h / 0 °C

17.1: 14.1 mg / potassium tert-butoxide / tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; dmap; lithium hydroxide; osmium(VIII) oxide; n-butyllithium; diphenylphosphoranyl azide; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; diisopropylamine; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00436-2

Reference yield:

: 159638-73-0
8-(2'-propenyl)-1,4-dioxaspiro[4.5]decane-8-carboxylic acid

: 211430-52-3
C₂₆H₃₄N₂O₄

Guidance literature:: Multi-step reaction with 16 steps

1.1: diphenylphosphoryl azide; triethylamine / benzene / 0.5 h / Heating

1.2: 65 percent / benzene / 5 h / Heating

2.1: 94 percent / osmium tetroxide; N-methylmorpholine N-oxide / acetone; H₂O; 2-methyl-propan-2-ol / 5 h / 20 °C

3.1: 86 percent / 4-(N,N-dimethylamino)pyridine / pyridine / 4 h / 20 °C

4.1: 92 percent / imidazole / dimethylformamide / 4.5 h / 20 °C

5.1: H₂ / 5 percent Pd/C / methanol / 3 h

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / benzene / 3.5 h / Heating

7.1: potassium carbonate / acetonitrile / 2.5 h / 20 °C

8.1: 964 mg / tetrabutylammonium fluoride / tetrahydrofuran / 15 h / 20 °C

9.1: 82 percent / diphenylphosphoryl azide; triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 2 h / 20 °C

10.1: 75 percent / H₂ / 5 percent Pd/C / methanol / 1.5 h

11.1: lithium hydroxide / H₂O / 0.67 h / 20 °C

12.1: 234 mg / diphenylphosphoryl azide; triethylamine / dimethylformamide / 1.5 h / 20 °C

13.1: 56 percent / sodium hydride / tetrahydrofuran / 1.5 h / 20 °C

14.1: lithium diisopropylamide / tetrahydrofuran / 0.33 h / -78 °C

14.2: 85 percent / tetrahydrofuran / 0.33 h / -78 °C

15.1: triethylamine / CH₂Cl₂ / 1 h / 0 °C

16.1: 14.1 mg / potassium tert-butoxide / tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; dmap; lithium hydroxide; osmium(VIII) oxide; diphenylphosphoranyl azide; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00436-2

Reference yield:

: 211430-44-3
11-(tert-Butyl-dimethyl-silanyloxy)-1,4-dioxa-9-aza-dispiro[4.2.4.2]tetradecane

: 211430-52-3
C₂₆H₃₄N₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / acetonitrile / 2.5 h / 20 °C

2.1: 964 mg / tetrabutylammonium fluoride / tetrahydrofuran / 15 h / 20 °C

3.1: 82 percent / diphenylphosphoryl azide; triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 2 h / 20 °C

4.1: 75 percent / H₂ / 5 percent Pd/C / methanol / 1.5 h

5.1: lithium hydroxide / H₂O / 0.67 h / 20 °C

6.1: 234 mg / diphenylphosphoryl azide; triethylamine / dimethylformamide / 1.5 h / 20 °C

7.1: 56 percent / sodium hydride / tetrahydrofuran / 1.5 h / 20 °C

8.1: lithium diisopropylamide / tetrahydrofuran / 0.33 h / -78 °C

8.2: 85 percent / tetrahydrofuran / 0.33 h / -78 °C

9.1: triethylamine / CH₂Cl₂ / 1 h / 0 °C

10.1: 14.1 mg / potassium tert-butoxide / tetrahydrofuran / 1 h / 0 °C

With lithium hydroxide; diphenylphosphoranyl azide; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; potassium carbonate; triethylamine; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(02)00436-2