2-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:853335-26-9
Molecular Formula:C₁₇H₂₃BO₃
Molecular Weight:286.179
Hs Code.:

Synonyms:2-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 2 articles about 2-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: tributyl((1E,3E)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)buta-1,3-dienyl)stannane

: 696-62-8
para-iodoanisole

: 853335-26-9
2-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; P(furyl)3; In 1-methyl-pyrrolidin-2-one; at 23 ℃; for 24h;
DOI:10.1021/ol050768u

Reference yield:

: 696-62-8
para-iodoanisole

: 81925-30-6,149538-53-4,219726-39-3
(E)-3-(tri-n-butylstannyl)-2-propenal

: 83622-41-7
pinacol dichloromethylboronic ester

: 853335-26-9
2-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: (E)-3-(tri-n-butylstannyl)-2-propenal; pinacol dichloromethylboronic ester; With chromium dichloride; lithium iodide; In tetrahydrofuran; at 23 ℃; for 3h;

para-iodoanisole; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; P(furyl)3; In 1-methyl-pyrrolidin-2-one; at 23 ℃; for 24h;
DOI:10.1021/ol050768u

Reference yield: 94.0%

: 853335-26-9
2-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 35779-04-5
1-tert-butyl-4-iodobenzene

: 1-tert-butyl-4-((1E,3E)-4-(4-methoxyphenyl)buta-1,3-dienyl)benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 50 ℃; for 16h;
DOI:10.1021/ol050768u