7-[(Benzyloxy)carbonyl]-3-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-5,6,7,8-tetrahydro[1,2,4]triazolo[4,3-a]pyrazin-1-ium Trifluoroacetate

Base Information

Chemical Name:7-[(Benzyloxy)carbonyl]-3-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-5,6,7,8-tetrahydro[1,2,4]triazolo[4,3-a]pyrazin-1-ium Trifluoroacetate
CAS No.:959841-70-4
Molecular Formula:C₂HF₃O₂*C₂₁H₂₉N₅O₄
Molecular Weight:529.516
Hs Code.:

Synonyms:7-[(Benzyloxy)carbonyl]-3-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-5,6,7,8-tetrahydro[1,2,4]triazolo[4,3-a]pyrazin-1-ium Trifluoroacetate

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Chemical Property of 7-[(Benzyloxy)carbonyl]-3-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-5,6,7,8-tetrahydro[1,2,4]triazolo[4,3-a]pyrazin-1-ium Trifluoroacetate

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Technology Process of 7-[(Benzyloxy)carbonyl]-3-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-5,6,7,8-tetrahydro[1,2,4]triazolo[4,3-a]pyrazin-1-ium Trifluoroacetate

There total 4 articles about 7-[(Benzyloxy)carbonyl]-3-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-5,6,7,8-tetrahydro[1,2,4]triazolo[4,3-a]pyrazin-1-ium Trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 959841-68-0
Benzyl 5-(2-{2-[(tert-butoxycarbonyl)amino]-2-methylpropanoyl}hydrazino)-3,6-dihydropyrazine-1(2H)-carboxylate

: 959841-70-4
7-[(Benzyloxy)carbonyl]-3-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-5,6,7,8-tetrahydro[1,2,4]triazolo[4,3-a]pyrazin-1-ium Trifluoroacetate

Guidance literature:: In methanol; w-BuOH; water; acetonitrile;

Reference yield:

: 30992-29-1
Boc-Aib-OH

: 959841-70-4
7-[(Benzyloxy)carbonyl]-3-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-5,6,7,8-tetrahydro[1,2,4]triazolo[4,3-a]pyrazin-1-ium Trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; methyl iodide / N,N-dimethyl-formamide

2: hydrazine hydrate / isopropyl alcohol

3: 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran

4: methanol; w-BuOH; water; acetonitrile

With potassium carbonate; hydrazine hydrate; methyl iodide; In methanol; w-BuOH; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;

Reference yield:

: 84758-55-4
N-(tert-butoxycarbonyl)-α-methylalanine methyl ester

: 959841-70-4
7-[(Benzyloxy)carbonyl]-3-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-5,6,7,8-tetrahydro[1,2,4]triazolo[4,3-a]pyrazin-1-ium Trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / isopropyl alcohol

2: 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran

3: methanol; w-BuOH; water; acetonitrile

With hydrazine hydrate; In methanol; w-BuOH; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; isopropyl alcohol; acetonitrile;