2(C₆H₅)4P⁽¹⁺⁾*((C₆H₅S)2FeS₂WS₂)^(2-)=((C₆H₅)4P)2((C₆H₅S)2FeS₂WS₂)

Base Information

Chemical Name:2(C₆H₅)4P⁽¹⁺⁾*((C₆H₅S)2FeS₂WS₂)^(2-)=((C₆H₅)4P)2((C₆H₅S)2FeS₂WS₂)
CAS No.:73493-04-6
Molecular Formula:C₁₂H₁₀FeS₆W*2C₂₄H₂₀P
Molecular Weight:1265.1
Hs Code.:

2(C<sub>6</sub>H<sub>5</sub>)4P<sup>(1+)</sup>*((C<sub>6</sub>H<sub>5</sub>S)2FeS<sub>2</sub>WS<sub>2</sub>)<sup>(2-)</sup>=((C<sub>6</sub>H<sub>5</sub>)4P)2((C<sub>6</sub>H<sub>5</sub>S)2FeS<sub>2</sub>WS<sub>2</sub>)

Synonyms:2(C₆H₅)4P⁽¹⁺⁾*((C₆H₅S)2FeS₂WS₂)^(2-)=((C₆H₅)4P)2((C₆H₅S)2FeS₂WS₂)

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Chemical Property of 2(C₆H₅)4P⁽¹⁺⁾*((C₆H₅S)2FeS₂WS₂)^(2-)=((C₆H₅)4P)2((C₆H₅S)2FeS₂WS₂)

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Technology Process of 2(C₆H₅)4P⁽¹⁺⁾*((C₆H₅S)2FeS₂WS₂)^(2-)=((C₆H₅)4P)2((C₆H₅S)2FeS₂WS₂)

There total 1 articles about 2(C₆H₅)4P⁽¹⁺⁾*((C₆H₅S)2FeS₂WS₂)^(2-)=((C₆H₅)4P)2((C₆H₅S)2FeS₂WS₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 13862-78-7
ammonium tetrathiotungstate

: 2P(C₆H₅)4⁽¹⁺⁾*Fe(S(C₆H₅))4^(2-)=(P(C₆H₅)4)2Fe(S(C₆H₅))4

: 73493-04-6
2(C₆H₅)4P⁽¹⁺⁾*((C₆H₅S)2FeS₂WS₂)^(2-)=((C₆H₅)4P)2((C₆H₅S)2FeS₂WS₂)

Guidance literature:: In N,N-dimethyl-formamide; to soln. of Fe complex was added soln. of W complex; stirring for 5 min; filtration, treating with EtOH and Et2O; filtration, washing with Et2O,drying in vac.; elem. anal.;

Reference yield: 92.0%

: 73493-04-6
2(C₆H₅)4P⁽¹⁺⁾*((C₆H₅S)2FeS₂WS₂)^(2-)=((C₆H₅)4P)2((C₆H₅S)2FeS₂WS₂)

: 6493-73-8
dibenzyltrisulfide

: 83560-84-3
(PPh₄)2[S₅FeS₂WS₂]*0.5DMF

Guidance literature:: In N,N-dimethyl-formamide; to soln. of complex was added soln. of Bn2S3; heating at ca 80°Cfor 5 min; filtration, adding of Et2O, standing for 0.5 h, filtration; elem. anal.;

Reference yield: 84.0%

: 121714-78-1,24290-40-2,58694-80-7,10025-77-1,64333-00-2
iron(III) chloride hexahydrate

: 73493-04-6
2(C₆H₅)4P⁽¹⁺⁾*((C₆H₅S)2FeS₂WS₂)^(2-)=((C₆H₅)4P)2((C₆H₅S)2FeS₂WS₂)

: 73621-81-5
2(C₆H₅)4P⁽¹⁺⁾*Cl₂WS₂FeS₂FeCl₂^(2-)=((C₆H₅)4P)2[Cl₂WS₂FeS₂FeCl₂]

Guidance literature:: In acetonitrile; under N2 atm. to soln. (Ph4P)2((PhS)2FeS2WS2) in CH3CN added soln. FeCl3*6H2O in CH3CN and soln. stirred for 10 min; soln. filtered, abs. ethanol added, Et2O added, crystals isolated by filtration, washed with Et2O and dried in vacuo; elem. anal.;