benzyl (2-(N-(4-chlorobenzyl)-2,2,2-trifluoroacetamido)cyclopent-2-en-1-yl)carbamate

Base Information

Chemical Name:benzyl (2-(N-(4-chlorobenzyl)-2,2,2-trifluoroacetamido)cyclopent-2-en-1-yl)carbamate
CAS No.:1391090-04-2
Molecular Formula:C₂₂H₂₀ClF₃N₂O₃
Molecular Weight:452.861
Hs Code.:

Synonyms:benzyl (2-(N-(4-chlorobenzyl)-2,2,2-trifluoroacetamido)cyclopent-2-en-1-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (2-(N-(4-chlorobenzyl)-2,2,2-trifluoroacetamido)cyclopent-2-en-1-yl)carbamate

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Technology Process of benzyl (2-(N-(4-chlorobenzyl)-2,2,2-trifluoroacetamido)cyclopent-2-en-1-yl)carbamate

There total 2 articles about benzyl (2-(N-(4-chlorobenzyl)-2,2,2-trifluoroacetamido)cyclopent-2-en-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1391090-18-8
1-(4-chlorophenyl)-N-cyclopentylidenemethanamine oxide

: 1391089-95-4
C₁₀H₇ClF₃NO₂

: 1391090-04-2
benzyl (2-(N-(4-chlorobenzyl)-2,2,2-trifluoroacetamido)cyclopent-2-en-1-yl)carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere; Cooling with ice;
DOI:10.1039/c2cc33401a

Reference yield:

: 51307-68-7
N-4-chlorobenzylhydroxylamine

: 120-92-3
cyclopentanone

: 1391090-04-2
benzyl (2-(N-(4-chlorobenzyl)-2,2,2-trifluoroacetamido)cyclopent-2-en-1-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: tert-butyl alcohol / 14 h / 110 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Cooling with ice

With triethylamine; In dichloromethane; tert-butyl alcohol; 2: Cope rearrangement;
DOI:10.1039/c2cc33401a