1-benzhydryl-3,3-dinitroazetidine

Base Information

Chemical Name:1-benzhydryl-3,3-dinitroazetidine
CAS No.:125735-39-9
Molecular Formula:C₁₆H₁₅N₃O₄
Molecular Weight:313.313
Hs Code.:

Synonyms:1-benzhydryl-3,3-dinitroazetidine

Suppliers and Price of 1-benzhydryl-3,3-dinitroazetidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzhydryl-3,3-dinitroazetidine

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Technology Process of 1-benzhydryl-3,3-dinitroazetidine

There total 2 articles about 1-benzhydryl-3,3-dinitroazetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 125735-37-7
1-benzhydryl-3-nitroazetidine

: 125735-39-9
1-benzhydryl-3,3-dinitroazetidine

Guidance literature:: With sodium hydroxide; tetranitromethane; sodium nitrite; In ethanol; for 0.5h;
DOI:10.1021/jo00296a066

Reference yield:

: 33301-41-6
1-benzhydryl-3-azetidinyl methanesulfonate

: 125735-39-9
1-benzhydryl-3,3-dinitroazetidine

Guidance literature:: Multi-step reaction with 2 steps

1: 11 percent / NaNO₂, NaI, phloroglucinol dihydrate / dimethylformamide; H₂O / 48 h / 50 °C

2: 38 percent / NaOH, NaNO₂, tetranitromethane / ethanol / 0.5 h

With sodium hydroxide; 3,5-dihydroxyphenol; tetranitromethane; sodium iodide; sodium nitrite; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00296a066