1-(bis(2,4,6-triisopropylphenyl)germyl)-1-mesityl-4,6-dimethyl-1-siladihydrobenzocyclobutene

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Chemical Name:1-(bis(2,4,6-triisopropylphenyl)germyl)-1-mesityl-4,6-dimethyl-1-siladihydrobenzocyclobutene
CAS No.:141376-96-7
Molecular Formula:C₄₈H₆₈GeSi
Molecular Weight:745.743
Hs Code.:

Synonyms:1-(bis(2,4,6-triisopropylphenyl)germyl)-1-mesityl-4,6-dimethyl-1-siladihydrobenzocyclobutene

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Chemical Property of 1-(bis(2,4,6-triisopropylphenyl)germyl)-1-mesityl-4,6-dimethyl-1-siladihydrobenzocyclobutene

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Technology Process of 1-(bis(2,4,6-triisopropylphenyl)germyl)-1-mesityl-4,6-dimethyl-1-siladihydrobenzocyclobutene

There total 1 articles about 1-(bis(2,4,6-triisopropylphenyl)germyl)-1-mesityl-4,6-dimethyl-1-siladihydrobenzocyclobutene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 141376-88-7
(chlorodimesitylsilyl)bis(2,4,6-triisopropylphenyl)germane

: 141376-96-7
1-(bis(2,4,6-triisopropylphenyl)germyl)-1-mesityl-4,6-dimethyl-1-siladihydrobenzocyclobutene

Guidance literature:: With hydrogenchloride; methanol; tert.-butyl lithium; In cyclohexane; addn. of t-BuLi in pentanes to a soln. of the silylgermane in cyclohexane at 10°C under dry Ar, warming, refluxing (3 h), cooling the dark orange soln., addn. of excess MeOH, color change to lemon yellow, stirring (1 h), hydrolysis (1 M HCl); extg. (Et2O), drying (over MgSO4), filtration, removing solvent, chromy.;
DOI:10.1021/om00042a035