N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Base Information

Chemical Name:N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside
CAS No.:1335110-88-7
Molecular Formula:C₆₆H₆₇Cl₃N₂O₁₈Si
Molecular Weight:1310.71
Hs Code.:

N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Synonyms:N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

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Chemical Property of N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

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Technology Process of N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

There total 1 articles about N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1159991-77-1
N-hydroxypent-4-enamide

: 1335110-87-6
C₆₉H₆₄Cl₃F₃N₂O₁₇Si

: 1335110-88-7
N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 20 ℃; for 1.5h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja206023e

Reference yield:

: 1335110-88-7
N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

: 1335110-89-8
N-hydroxypent-4-enamide (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-6-O-(tert-butyldiphenylsilyl)-3-O-acetyl-2-deoxy-2-acetamido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid; zinc / acetonitrile / 3 h / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / methanol / 1.5 h / 0 °C / Inert atmosphere

With formic acid; N-ethyl-N,N-diisopropylamine; zinc; In methanol; acetonitrile;
DOI:10.1021/ja206023e