C₃₄H₂₂O₂

Base Information

Chemical Name:C₃₄H₂₂O₂
CAS No.:1136522-55-8
Molecular Formula:C₃₄H₂₂O₂
Molecular Weight:462.547
Hs Code.:

C<sub>34</sub>H<sub>22</sub>O<sub>2</sub>

Synonyms:C₃₄H₂₂O₂

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Chemical Property of C₃₄H₂₂O₂

Chemical Property:

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Technology Process of C₃₄H₂₂O₂

There total 5 articles about C₃₄H₂₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 86-73-7
9H-fluorene

: 1136522-53-6
C₂₁H₁₃BrO₂

: 1136522-55-8
C₃₄H₂₂O₂

Guidance literature:: 9H-fluorene; With potassium tert-butylate; In ISOPROPYLAMIDE; for 0.0833333h; Inert atmosphere;

C₂₁H₁₃BrO₂; In ISOPROPYLAMIDE; at 20 ℃; for 1.16667h;

With hydrogenchloride; water; In ISOPROPYLAMIDE; Inert atmosphere; Cooling with ice;
DOI:10.1021/ol9001575

Reference yield:

: 1136522-52-5
C₂₁H₁₄Br₂O₂

: 1136522-55-8
C₃₄H₂₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol / Reflux

2.1: potassium tert-butylate / N,N-dimethyl acetamide / Schlenk technique

2.2: 20 °C / Schlenk technique

With potassium tert-butylate; sodium hydroxide; In ethanol; N,N-dimethyl acetamide;
DOI:10.1039/c4ob02356k

Reference yield:

: 86-73-7
9H-fluorene

: 1136522-55-8
C₃₄H₂₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / ethanol / 16 h / Reflux

2.1: bromine / tetrachloromethane / 0.17 h / 20 °C

3.1: sodium hydroxide / ethanol / Reflux

4.1: potassium tert-butylate / N,N-dimethyl acetamide / Schlenk technique

4.2: 20 °C / Schlenk technique

With potassium tert-butylate; bromine; sodium hydroxide; In tetrachloromethane; ethanol; N,N-dimethyl acetamide;
DOI:10.1039/c4ob02356k