3-acetamido-5-azidobenzoic acid

Base Information

Chemical Name:3-acetamido-5-azidobenzoic acid
CAS No.:1452402-90-2
Molecular Formula:C₉H₈N₄O₃
Molecular Weight:220.188
Hs Code.:

Synonyms:3-acetamido-5-azidobenzoic acid

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Chemical Property of 3-acetamido-5-azidobenzoic acid

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Technology Process of 3-acetamido-5-azidobenzoic acid

There total 5 articles about 3-acetamido-5-azidobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1452402-89-9
methyl 3-acetamido-5-azidobenzoate

: 1452402-90-2
3-acetamido-5-azidobenzoic acid

Guidance literature:: With lithium hydroxide; In methanol; at 50 ℃;
DOI:10.1021/ol401989e

Reference yield:

: 23218-93-1
3-amino-5-nitro-benzoic acid methyl ester

: 1452402-90-2
3-acetamido-5-azidobenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 1,4-dioxane / 19 h / 20 °C

2.1: tin(II) chloride dihdyrate / ethyl acetate / Reflux

3.1: sodium nitrite; hydrogenchloride / water / 6 h / -5 °C

3.2: 12 h / 20 °C

4.1: lithium hydroxide / methanol / 50 °C

With pyridine; hydrogenchloride; tin(II) chloride dihdyrate; lithium hydroxide; sodium nitrite; In 1,4-dioxane; methanol; water; ethyl acetate;
DOI:10.1021/ol401989e

Reference yield:

: 618-84-8
3-amino-5-nitro-benzoic acid

: 1452402-90-2
3-acetamido-5-azidobenzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetyl chloride / 48 h / 80 °C

2.1: pyridine / 1,4-dioxane / 19 h / 20 °C

3.1: tin(II) chloride dihdyrate / ethyl acetate / Reflux

4.1: sodium nitrite; hydrogenchloride / water / 6 h / -5 °C

4.2: 12 h / 20 °C

5.1: lithium hydroxide / methanol / 50 °C

With pyridine; hydrogenchloride; tin(II) chloride dihdyrate; acetyl chloride; lithium hydroxide; sodium nitrite; In 1,4-dioxane; methanol; water; ethyl acetate;
DOI:10.1021/ol401989e