(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylsulfonylpentane

Base Information

Chemical Name:(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylsulfonylpentane
CAS No.:123387-99-5
Molecular Formula:C₃₈H₄₈O₆SSi
Molecular Weight:660.947
Hs Code.:

Synonyms:(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylsulfonylpentane

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Chemical Property of (2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylsulfonylpentane

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Technology Process of (2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylsulfonylpentane

There total 4 articles about (2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylsulfonylpentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 131755-74-3
(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylthiopentane

: 123387-99-5
(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylsulfonylpentane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 0.75h;
DOI:10.1016/S0040-4020(01)85585-X

Reference yield:

: 124582-88-3
(2S,3R,4S)-5-(tert-Butyl-diphenyl-silanyloxy)-3-(3,4-dimethoxy-benzyloxy)-2,4-dimethyl-pentan-1-ol

: 123387-99-5
(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylsulfonylpentane

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / CH₂Cl₂ / 14 h / Ambient temperature

2: 89 percent / NaH / tetrahydrofuran; dimethylformamide / 0.75 h / Ambient temperature

3: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 0.75 h

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85585-X

Reference yield:

: 131755-73-2
(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-methylsulfonyloxypentane

: 123387-99-5
(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylsulfonylpentane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NaH / tetrahydrofuran; dimethylformamide / 0.75 h / Ambient temperature

2: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 0.75 h

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85585-X