methyl 6-(4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamido)hexanoate

Base Information

Chemical Name:methyl 6-(4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamido)hexanoate
CAS No.:1445854-52-3
Molecular Formula:C₃₂H₄₇NO₅
Molecular Weight:525.729
Hs Code.:

Synonyms:methyl 6-(4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamido)hexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-(4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamido)hexanoate

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Technology Process of methyl 6-(4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamido)hexanoate

There total 11 articles about methyl 6-(4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamido)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 700833-20-1
4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)-pentan-3-yl)benzoic acid

: 17994-94-4
methyl 7-aminoheptanoate hydrochloride

: 1445854-52-3
methyl 6-(4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamido)hexanoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2015.05.011

Reference yield: 58.0%

: 700833-20-1
4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)-pentan-3-yl)benzoic acid

methyl 6-aminohexanoate hydrochloride: 2780-89-4
methyl 6-aminohexanoate hydrochloride

: 1445854-52-3
methyl 6-(4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamido)hexanoate

Guidance literature:: With dmap; triethylamine; dicyclohexyl-carbodiimide; Inert atmosphere;

Reference yield:

: 1445854-36-3
3-(4-(benzyloxy)phenyl)pentan-3-ol

: 1445854-52-3
methyl 6-(4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamido)hexanoate

Guidance literature:: Multi-step reaction with 8 steps

1: boron trifluoride diethyl etherate / Inert atmosphere

2: potassium carbonate / Inert atmosphere

3: palladium; hydrogen

4: triethylamine; dmap / Inert atmosphere

5: triethylamine; palladium diacetate; triphenylphosphine / Inert atmosphere

6: sodium tetrahydroborate / Inert atmosphere

7: potassium hydroxide / Inert atmosphere

8: triethylamine; dmap; dicyclohexyl-carbodiimide / Inert atmosphere

With dmap; sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen; palladium diacetate; potassium carbonate; palladium; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide;