C₅₂H₈₂O₁₀Si₃

Base Information

Chemical Name:C₅₂H₈₂O₁₀Si₃
CAS No.:945468-73-5
Molecular Formula:C₅₂H₈₂O₁₀Si₃
Molecular Weight:951.474
Hs Code.:

C<sub>52</sub>H<sub>82</sub>O<sub>10</sub>Si<sub>3</sub>

Synonyms:C₅₂H₈₂O₁₀Si₃

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Chemical Property of C₅₂H₈₂O₁₀Si₃

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Technology Process of C₅₂H₈₂O₁₀Si₃

There total 31 articles about C₅₂H₈₂O₁₀Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 945468-72-4
C₆₁H₉₂O₁₂Si₃

: 945468-73-5
C₅₂H₈₂O₁₀Si₃

Guidance literature:: With 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: C₁₇H₂₄O₅

: 945468-73-5
C₅₂H₈₂O₁₀Si₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: 73 percent / DIBALH / CH₂Cl₂ / 0.67 h / -78 °C

2.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

3.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

4.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

5.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

6.1: 87 percent / TPAP; NMO; 4A MS / CH₂Cl₂ / 0.5 h / 0 °C

7.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

7.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

8.1: 98 percent / NaBH₄; CeCl₃*H₂O / ethanol / 3 h / -20 °C

9.1: 93 percent / K₂CO₃ / methanol / 2 h / 24 °C

10.1: 95 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 2 h / 0 °C

11.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -20 °C

12.1: 77 percent / CSA / CH₂Cl₂ / 4 h / 0 °C

13.1: 95 percent / pyridine / CH₂Cl₂ / 2 h / 0 °C

14.1: 95 percent / TMSOTf; 2,6-lutidine / CH₂Cl₂ / 2 h / 0 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; lithium aluminium tetrahydride; N-methyl-2-indolinone; cerium(III) chloride; tetrapropylammonium perruthennate; L-(+)-diisopropyl tartrate; trimethylsilyl trifluoromethanesulfonate; camphor-10-sulfonic acid; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; 4A MS; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene; 2.1: Katsuki-Sharpless asymmetric epoxidation / 7.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-63-3
C₁₅H₂₂O₄

: 945468-73-5
C₅₂H₈₂O₁₀Si₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

2.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

3.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

4.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

5.1: 87 percent / TPAP; NMO; 4A MS / CH₂Cl₂ / 0.5 h / 0 °C

6.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

6.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

7.1: 98 percent / NaBH₄; CeCl₃*H₂O / ethanol / 3 h / -20 °C

8.1: 93 percent / K₂CO₃ / methanol / 2 h / 24 °C

9.1: 95 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 2 h / 0 °C

10.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -20 °C

11.1: 77 percent / CSA / CH₂Cl₂ / 4 h / 0 °C

12.1: 95 percent / pyridine / CH₂Cl₂ / 2 h / 0 °C

13.1: 95 percent / TMSOTf; 2,6-lutidine / CH₂Cl₂ / 2 h / 0 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; lithium aluminium tetrahydride; N-methyl-2-indolinone; cerium(III) chloride; tetrapropylammonium perruthennate; L-(+)-diisopropyl tartrate; trimethylsilyl trifluoromethanesulfonate; camphor-10-sulfonic acid; sodium hydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; 4A MS; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene; 1.1: Katsuki-Sharpless asymmetric epoxidation / 6.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136