[CuCl₂(2-(bis(pyridin-2-ylmethyl)amino)-N-[(2,2-diphenyl-ethylcarbamoyl)methyl]acetamide)]*(C(O)NHCH₂C₆H₄)4 rotaxane

Base Information

• Chemical Name: [CuCl₂(2-(bis(pyridin-2-ylmethyl)amino)-N-[(2,2-diphenyl-ethylcarbamoyl)methyl]acetamide)]*(C(O)NHCH₂C₆H₄)4 rotaxane
• CAS No.: 876289-61-1
• Molecular Formula: C₃₀H₃₁Cl₂CuN₅O₂*C₃₂H₂₈N₄O₄
• Molecular Weight: 1160.66

Synonyms:[CuCl₂(2-(bis(pyridin-2-ylmethyl)amino)-N-[(2,2-diphenyl-ethylcarbamoyl)methyl]acetamide)]*(C(O)NHCH₂C₆H₄)4 rotaxane

Chemical Property of [CuCl₂(2-(bis(pyridin-2-ylmethyl)amino)-N-[(2,2-diphenyl-ethylcarbamoyl)methyl]acetamide)]*(C(O)NHCH₂C₆H₄)4 rotaxane

Chemical Property:

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Technology Process of [CuCl₂(2-(bis(pyridin-2-ylmethyl)amino)-N-[(2,2-diphenyl-ethylcarbamoyl)methyl]acetamide)]*(C(O)NHCH₂C₆H₄)4 rotaxane

There total 1 articles about [CuCl₂(2-(bis(pyridin-2-ylmethyl)amino)-N-[(2,2-diphenyl-ethylcarbamoyl)methyl]acetamide)]*(C(O)NHCH₂C₆H₄)4 rotaxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

([2](1,7,14,20-tetraaza-2,6,15,19-tetraoxo-3,5,9,12,16,18,22,25-tetrabenzocyclohexacosane)-(2-(bis-pyridin-2-ylmethyl-amino)-N-[(2,2-diphenylethylcarbamoyl)-methyl]-acetamide)) rotaxane (876289-68-8) + copper(II) choride dihydrate → [CuCl2(2-(bis(pyridin-2-ylmethyl)amino)-N-[(2,2-diphenyl-ethylcarbamoyl)methyl]acetamide)]*(C(O)NHCH2C6H4)4 rotaxane (876289-61-1)

Guidance literature:

In not given; CuCl2*2H2O added to ((C5NH4)CH2)2N(CH2C(O)NH)2CH2CH(C6H5)2*(C(O)NHCH2C6H4)4;

DOI:10.1002/anie.200501761

Reference yield:

[CuCl2(2-(bis(pyridin-2-ylmethyl)amino)-N-[(2,2-diphenyl-ethylcarbamoyl)methyl]acetamide)]*(C(O)NHCH2C6H4)4 rotaxane (876289-61-1) → [CuCl(2-(bis(pyridin-2-ylmethyl)amino)-N-[(2,2-diphenyl-ethylcarbamoyl)methyl]acetamide)]*(C(O)NHCH2C6H4)4 rotaxane

Guidance literature:

With NaH or phosphazene P₁-tBu base; In not given; 1 equiv. of NaH (or N'-tert-butyl-N,N,N',N',N'',N''-hexamethylphosphorimidic triamide) added to (CuCl2((C5NH4)CH2)2N(CH2C(O)NH)2CH2CH(C6H5)2)*(C(O)NHCH2C6H4)4);

DOI:10.1002/anie.200501761

upstream raw materials:

([2](1,7,14,20-tetraaza-2,6,15,19-tetraoxo-3,5,9,12,16,18,22,25-tetrabenzocyclohexacosane)-(2-(bis-pyridin-2-ylmethyl-amino)-N-[(2,2-diphenylethylcarbamoyl)-methyl]-acetamide)) rotaxane

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