2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-4-pentenoic acid

Base Information

Chemical Name:2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-4-pentenoic acid
CAS No.:796072-01-0
Molecular Formula:C₃₄H₃₁NO₅
Molecular Weight:533.624
Hs Code.:

Synonyms:2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-4-pentenoic acid

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Chemical Property of 2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-4-pentenoic acid

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Technology Process of 2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-4-pentenoic acid

There total 9 articles about 2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-4-pentenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 796072-31-6
2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-5-pentenoic acid methyl ester

: 796072-01-0
2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-4-pentenoic acid

Guidance literature:: With potassium hydroxide; water; In tetrahydrofuran; methanol; at 20 ℃; for 1h;

Reference yield:

: 796072-24-7
(4-dibenzofuran-4-yl-phenyl)-trimethyl-silane

: 796072-01-0
2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-4-pentenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron tribromide / dichloromethane / 3 h / -78 - 20 °C

1.2: 2.5 h / -78 - 20 °C

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 2 h / Heating / reflux

3.1: potassium hydroxide; water / tetrahydrofuran; methanol / 1 h / 20 °C

With potassium hydroxide; water; boron tribromide; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 2.1: Suzuki Coupling;

Reference yield:

: 796071-96-0
(4-(dibenzo[b,d]furan-4-yl)phenyl)boronic acid

: 796072-01-0
2-tert-butoxycarbonylamino-5-(4'-dibenzofuran-4-yl-biphen-4-yl)-4-pentenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 2 h / Heating / reflux

2: potassium hydroxide; water / tetrahydrofuran; methanol / 1 h / 20 °C

With potassium hydroxide; water; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; water; toluene; 1: Suzuki Coupling;