Benzyl-2-acetamido-3-O-acetyl-2,4-didesoxy-β-L-threo-hex-4-enopyranosiduronsaeure-methylester

Base Information

Chemical Name:Benzyl-2-acetamido-3-O-acetyl-2,4-didesoxy-β-L-threo-hex-4-enopyranosiduronsaeure-methylester
CAS No.:136409-07-9
Molecular Formula:C₁₈H₂₁NO₇
Molecular Weight:363.367
Hs Code.:

Synonyms:Benzyl-2-acetamido-3-O-acetyl-2,4-didesoxy-β-L-threo-hex-4-enopyranosiduronsaeure-methylester

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Chemical Property of Benzyl-2-acetamido-3-O-acetyl-2,4-didesoxy-β-L-threo-hex-4-enopyranosiduronsaeure-methylester

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Technology Process of Benzyl-2-acetamido-3-O-acetyl-2,4-didesoxy-β-L-threo-hex-4-enopyranosiduronsaeure-methylester

There total 2 articles about Benzyl-2-acetamido-3-O-acetyl-2,4-didesoxy-β-L-threo-hex-4-enopyranosiduronsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 113091-56-8
methyl (benzyl 2-acetamido-3,4-di-O-acetyl-2-deoxy-α-D-glucopyranosid)uronate

: 136409-07-9
Benzyl-2-acetamido-3-O-acetyl-2,4-didesoxy-β-L-threo-hex-4-enopyranosiduronsaeure-methylester

Guidance literature:: With 7-methyl-1,3,5-triazabicyclo<4.4.0>dec-5-ene; 3 A molecular sieve; In toluene; for 1.83333h; Heating;

Reference yield: 31.0%

: 108-24-7
acetic anhydride

: 136409-08-0
Sodium; (2S,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-3,4-dihydroxy-tetrahydro-pyran-2-carboxylate

: 136409-07-9
Benzyl-2-acetamido-3-O-acetyl-2,4-didesoxy-β-L-threo-hex-4-enopyranosiduronsaeure-methylester

Guidance literature:: With cesium acetate; for 2h; Heating;

Reference yield:

: 136409-07-9
Benzyl-2-acetamido-3-O-acetyl-2,4-didesoxy-β-L-threo-hex-4-enopyranosiduronsaeure-methylester

: 136408-97-4
Methyl-2-acetamido-3-O-acetyl-2-desoxy-N-(4-methoxybenzyliden)-α-D-xylo-hexopyranuronatosylamin-N-oxid

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / H₂ / 10percent Pd/C / methanol / 48 h / 760 Torr

2: 1) hydroxylamine hydrochloride, 1 N NaOMe / 1) EtOH, 50 deg C, 2) 50 deg C, 1 h

3: 32 percent / CSA / 20 h / Ambient temperature

With camphor-10-sulfonic acid; hydroxylamine hydrochloride; hydrogen; sodium methylate; palladium on activated charcoal; In methanol;