1S-[3R,9R-bis(tert-butyldimethylsilanyloxy)-2R,8S,10S-trimethyl-1-(1S-methylpent-2Z-enyl)heptadeca-11Z,16-dienyloxymethyl]-4-methoxybenzene

Base Information

Chemical Name:1S-[3R,9R-bis(tert-butyldimethylsilanyloxy)-2R,8S,10S-trimethyl-1-(1S-methylpent-2Z-enyl)heptadeca-11Z,16-dienyloxymethyl]-4-methoxybenzene
CAS No.:1234501-37-1
Molecular Formula:C₄₆H₈₄O₄Si₂
Molecular Weight:757.342
Hs Code.:

1S-[3R,9R-bis(tert-butyldimethylsilanyloxy)-2R,8S,10S-trimethyl-1-(1S-methylpent-2Z-enyl)heptadeca-11Z,16-dienyloxymethyl]-4-methoxybenzene

Synonyms:1S-[3R,9R-bis(tert-butyldimethylsilanyloxy)-2R,8S,10S-trimethyl-1-(1S-methylpent-2Z-enyl)heptadeca-11Z,16-dienyloxymethyl]-4-methoxybenzene

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Chemical Property of 1S-[3R,9R-bis(tert-butyldimethylsilanyloxy)-2R,8S,10S-trimethyl-1-(1S-methylpent-2Z-enyl)heptadeca-11Z,16-dienyloxymethyl]-4-methoxybenzene

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Technology Process of 1S-[3R,9R-bis(tert-butyldimethylsilanyloxy)-2R,8S,10S-trimethyl-1-(1S-methylpent-2Z-enyl)heptadeca-11Z,16-dienyloxymethyl]-4-methoxybenzene

There total 1 articles about 1S-[3R,9R-bis(tert-butyldimethylsilanyloxy)-2R,8S,10S-trimethyl-1-(1S-methylpent-2Z-enyl)heptadeca-11Z,16-dienyloxymethyl]-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1234501-17-7
3R,9R-bis-(tert-butyldimethylsilanyloxy)-11S-(4-methoxybenzyloxy)-2R,4S,10R,12S-tetramethylhexadec-13Z-enal

: 102112-92-5
(hex-5-en-1-yl)triphenylphosphonium bromide

: 1234501-37-1
1S-[3R,9R-bis(tert-butyldimethylsilanyloxy)-2R,8S,10S-trimethyl-1-(1S-methylpent-2Z-enyl)heptadeca-11Z,16-dienyloxymethyl]-4-methoxybenzene

Guidance literature:: (hex-5-en-1-yl)triphenylphosphonium bromide; With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

3R,9R-bis-(tert-butyldimethylsilanyloxy)-11S-(4-methoxybenzyloxy)-2R,4S,10R,12S-tetramethylhexadec-13Z-enal; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja103537u