1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-sn-glycerol

Base Information

Chemical Name:1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-sn-glycerol
CAS No.:874141-07-8
Molecular Formula:C₃₁H₄₄O₅
Molecular Weight:496.687
Hs Code.:

Synonyms:1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-sn-glycerol

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Chemical Property of 1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-sn-glycerol

Chemical Property:

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Technology Process of 1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-sn-glycerol

There total 3 articles about 1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-3-O-(4-methoxyphenyl)-sn-glycerol

: 874141-07-8
1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-sn-glycerol

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile;
DOI:10.1021/jo052030w

Reference yield:

: 4-((Z)-bromotridec-4-enyl)benzophenone

: 874141-07-8
1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: 10 percent / cesium fluoride; 18-crown-6 / dimethylformamide / 24 h / 20 °C

2: 89 percent / i-Pr₂NEt / CH₂Cl₂

3: 88 percent / CAN / acetonitrile; H₂O

With ammonium cerium(IV) nitrate; 18-crown-6 ether; N-ethyl-N,N-diisopropylamine; cesium fluoride; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo052030w

Reference yield:

: 1027646-81-6
2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-3-O-(4-methoxyphenyl)-sn-glycerol

: 874141-07-8
1-O-methoxymethyl-2-O-(13-(4-benzoylphenyl)-9-(Z)-tridecenyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / i-Pr₂NEt / CH₂Cl₂

2: 88 percent / CAN / acetonitrile; H₂O

With ammonium cerium(IV) nitrate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; acetonitrile;
DOI:10.1021/jo052030w