Technology Process of C43H45N5O10
There total 12 articles about C43H45N5O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
2: dichloro-acetic acid / dichloromethane / 0.67 h / 20 °C / Inert atmosphere
With
4-methyl-morpholine; dichloro-acetic acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
DOI:10.1002/chem.201201662
DOI:10.1002/chem.201201662
- Guidance literature:
-
Multi-step reaction with 8 steps
1: sodium tetrachloropalladate(II) / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere
2: ammonium hydroxide / 5 h / 20 °C / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine / water; tetrahydrofuran / 0 - 20 °C / Inert atmosphere
4: pyridine / 20 °C / Inert atmosphere
5: 5 h / 20 °C / Inert atmosphere
6: piperidine / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
8: dichloro-acetic acid / dichloromethane / 0.67 h / 20 °C / Inert atmosphere
With
piperidine; 4-methyl-morpholine; pyridine; dichloro-acetic acid; ammonium hydroxide; sodium tetrachloropalladate(II); benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201201662
DOI:10.1002/chem.201201662