(+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester

Base Information

Chemical Name:(+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester
CAS No.:147503-33-1
Molecular Formula:C₂₂H₃₈N₂O₆
Molecular Weight:426.554
Hs Code.:

(+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis<butansaeure>-diethylester

Synonyms:(+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester

Suppliers and Price of (+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester

There total 4 articles about (+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 81430-18-4
3-(Chloroformyl)-3,3-dimethylbutansaeure-1-ethylester

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 147503-33-1
(+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester

Guidance literature:: With triethylamine; In tetrahydrofuran; 1) 0 deg C, 40 min, 2) RT, overnight;
DOI:10.1002/hlca.19930760120

Reference yield:

: 17347-61-4
2,2-dimethylsuccinic anhydride

: 147503-33-1
(+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 4 h / Heating

2: 97 percent / SOCl₂ / dimethylformamide / 3.5 h / 60 °C

3: 88 percent / NEt₃ / tetrahydrofuran / 1) 0 deg C, 40 min, 2) RT, overnight

With thionyl chloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19930760120

Reference yield:

: 597-43-3
2,2-dimethylsuccinic acid

: 147503-33-1
(+)-3,3'-(<(1R,2R)-Cyclohexan-1,2-diyl>bis(iminocarbonyl))-3,3'-dimethylbis-diethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / Ac₂O / 2 h / 160 °C

2: 76 percent / 4 h / Heating

3: 97 percent / SOCl₂ / dimethylformamide / 3.5 h / 60 °C

4: 88 percent / NEt₃ / tetrahydrofuran / 1) 0 deg C, 40 min, 2) RT, overnight

With thionyl chloride; acetic anhydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19930760120