N-[{(2S,5R,6S)-5-[2-{[N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6-methoxy-5,6-dihydro-2H-pyran-2-yl}methyl]-N-[(1S,4S)-4-hydroxycyclohept-2-en-1-yl]-2-nitrobenzenesulfonamide

Base Information

• Chemical Name: N-[{(2S,5R,6S)-5-[2-{[N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6-methoxy-5,6-dihydro-2H-pyran-2-yl}methyl]-N-[(1S,4S)-4-hydroxycyclohept-2-en-1-yl]-2-nitrobenzenesulfonamide
• CAS No.: 1252932-39-0
• Molecular Formula: C₄₁H₄₂F₁₇N₃O₁₀S₂
• Molecular Weight: 1123.9

Synonyms:N-[{(2S,5R,6S)-5-[2-{[N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6-methoxy-5,6-dihydro-2H-pyran-2-yl}methyl]-N-[(1S,4S)-4-hydroxycyclohept-2-en-1-yl]-2-nitrobenzenesulfonamide

Chemical Property of N-[{(2S,5R,6S)-5-[2-{[N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6-methoxy-5,6-dihydro-2H-pyran-2-yl}methyl]-N-[(1S,4S)-4-hydroxycyclohept-2-en-1-yl]-2-nitrobenzenesulfonamide

Chemical Property:

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Technology Process of N-[{(2S,5R,6S)-5-[2-{[N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6-methoxy-5,6-dihydro-2H-pyran-2-yl}methyl]-N-[(1S,4S)-4-hydroxycyclohept-2-en-1-yl]-2-nitrobenzenesulfonamide

There total 1 articles about N-[{(2S,5R,6S)-5-[2-{[N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6-methoxy-5,6-dihydro-2H-pyran-2-yl}methyl]-N-[(1S,4S)-4-hydroxycyclohept-2-en-1-yl]-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C43H44F17N3O11S2 (1252933-10-0) → N-[{(2S,5R,6S)-5-[2-{[N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6-methoxy-5,6-dihydro-2H-pyran-2-yl}methyl]-N-[(1S,4S)-4-hydroxycyclohept-2-en-1-yl]-2-nitrobenzenesulfonamide (1252932-39-0)

Guidance literature:

With ammonia; In methanol; at 20 ℃; for 48h;

DOI:10.1002/chem.201000707

Reference yield: 74.0%

N-(4-allyloxy-but-2-yn-1-yl)-2-nitrobenzenesulfonamide (1120367-45-4) + N-[{(2S,5R,6S)-5-[2-{[N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6-methoxy-5,6-dihydro-2H-pyran-2-yl}methyl]-N-[(1S,4S)-4-hydroxycyclohept-2-en-1-yl]-2-nitrobenzenesulfonamide (1252932-39-0) → N-[4-(allyloxy)but-2-ynyl]-N-[(1'R,4'S)-4'-{N'-[{(2''S,5''R,6''S)-5''-[2-{[N'-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6''-methoxy-5'',6''-dihydro-2H-pyran-2''-yl}methyl]-2-nitrophenylsulfonamido}cyclohept-2'-enyl]-2-nitrobenzenesulfonamide (1252932-61-8)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1002/chem.201000707

Reference yield: 67.0%

N-[{(2S,5R,6S)-5-[2-{[N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6-methoxy-5,6-dihydro-2H-pyran-2-yl}methyl]-N-[(1S,4S)-4-hydroxycyclohept-2-en-1-yl]-2-nitrobenzenesulfonamide (1252932-39-0) + N-allyl-o-nitrobenzenesulfonamide (65118-17-4) → N-allyl-N-[(1R,4S)-4-{N'-[{(2'S,5'R,6'S)-5'-[2-{[N''-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6'-methoxy-5',6'-dihydro-2H-pyran-2'-yl}methyl]-2-nitrophenylsulfonamido}cyclohept-2-enyl]-2-nitrobenzenesulfonamide (1252932-59-4)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1002/chem.201000707

upstream raw materials:

C₄₃H₄₄F₁₇N₃O₁₁S₂

Downstream raw materials:

N-[4-(allyloxy)but-2-ynyl]-N-[(1'R,4'S)-4'-{N'-[{(2''S,5''R,6''S)-5''-[2-{[N'-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6''-methoxy-5'',6''-dihydro-2H-pyran-2''-yl}methyl]-2-nitrophenylsulfonamido}cyclohept-2'-enyl]-2-nitrobenzenesulfonamide

C₅₁H₅₂F₁₇N₅O₁₃S₃

N-allyl-N-[(1R,4S)-4-{N'-[{(2'S,5'R,6'S)-5'-[2-{[N''-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy]-6'-methoxy-5',6'-dihydro-2H-pyran-2'-yl}methyl]-2-nitrophenylsulfonamido}cyclohept-2-enyl]-2-nitrobenzenesulfonamide

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