(Z)-N-(3,4-dimethoxybenzylidine)-1(R)-((S)-1,4-dioxaspiro[4,5]decane-2-yl)but-3-en-1-amine oxide

Base Information

Chemical Name:(Z)-N-(3,4-dimethoxybenzylidine)-1(R)-((S)-1,4-dioxaspiro[4,5]decane-2-yl)but-3-en-1-amine oxide
CAS No.:1333213-06-1
Molecular Formula:C₂₁H₂₉NO₅
Molecular Weight:375.465
Hs Code.:

Synonyms:(Z)-N-(3,4-dimethoxybenzylidine)-1(R)-((S)-1,4-dioxaspiro[4,5]decane-2-yl)but-3-en-1-amine oxide

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Chemical Property of (Z)-N-(3,4-dimethoxybenzylidine)-1(R)-((S)-1,4-dioxaspiro[4,5]decane-2-yl)but-3-en-1-amine oxide

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Technology Process of (Z)-N-(3,4-dimethoxybenzylidine)-1(R)-((S)-1,4-dioxaspiro[4,5]decane-2-yl)but-3-en-1-amine oxide

There total 4 articles about (Z)-N-(3,4-dimethoxybenzylidine)-1(R)-((S)-1,4-dioxaspiro[4,5]decane-2-yl)but-3-en-1-amine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1333213-04-9
N-(3,4-dimethoxybenzyl)-1(R)-((S)-1,4-dioxaspiro[4,5]decan-2-yl)but-3-en-1-amine

: 1333213-06-1
(Z)-N-(3,4-dimethoxybenzylidine)-1(R)-((S)-1,4-dioxaspiro[4,5]decane-2-yl)but-3-en-1-amine oxide

Guidance literature:: With sodium tungstate heptahydrate; dihydrogen peroxide; In water; acetone; for 12h; stereoselective reaction;
DOI:10.1021/ol2019967

Reference yield:

: 1333213-03-8
C₁₈H₂₅NO₄

: 1333213-06-1
(Z)-N-(3,4-dimethoxybenzylidine)-1(R)-((S)-1,4-dioxaspiro[4,5]decane-2-yl)but-3-en-1-amine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 12.5 h / -30 °C / Inert atmosphere

2: sodium tungstate heptahydrate; dihydrogen peroxide / water; acetone / 12 h

With sodium tungstate heptahydrate; dihydrogen peroxide; In diethyl ether; water; acetone;
DOI:10.1021/ol2019967

Reference yield:

: 78008-36-3
(R)-2,3-cyclohexylideneglyceraldehyde

: 1333213-06-1
(Z)-N-(3,4-dimethoxybenzylidine)-1(R)-((S)-1,4-dioxaspiro[4,5]decane-2-yl)but-3-en-1-amine oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium sulfate / tetrahydrofuran / 0.17 h / 5 °C / Inert atmosphere

1.2: 5 - 20 °C / Inert atmosphere

2.1: diethyl ether / 12.5 h / -30 °C / Inert atmosphere

3.1: sodium tungstate heptahydrate; dihydrogen peroxide / water; acetone / 12 h

With sodium tungstate heptahydrate; dihydrogen peroxide; magnesium sulfate; In tetrahydrofuran; diethyl ether; water; acetone;
DOI:10.1021/ol2019967