Technology Process of C30H56N2O2
There total 6 articles about C30H56N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 1h;
DOI:10.1016/j.tet.2010.11.046
- Guidance literature:
-
Multi-step reaction with 3 steps
1: nitric acid; acetic acid / chloroform / 0.25 h / 0 °C
2: tin(II) chloride hydrate / ethyl acetate / 2 h / Reflux
3: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C
With
sodium tetrahydroborate; tin(II) chloride hydrate; nitric acid; acetic acid;
In
tetrahydrofuran; methanol; chloroform; ethyl acetate;
DOI:10.1016/j.tet.2010.11.046
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / chloroform / 0 - 20 °C
2: nitric acid; acetic acid / chloroform / 0.25 h / 0 °C
3: tin(II) chloride hydrate / ethyl acetate / 2 h / Reflux
4: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C
With
sodium tetrahydroborate; tin(II) chloride hydrate; nitric acid; acetic acid; triethylamine;
In
tetrahydrofuran; methanol; chloroform; ethyl acetate;
DOI:10.1016/j.tet.2010.11.046