C₃₉H₄₅NO₃S₃Si

Base Information

Chemical Name:C₃₉H₄₅NO₃S₃Si
CAS No.:1261033-32-2
Molecular Formula:C₃₉H₄₅NO₃S₃Si
Molecular Weight:700.075
Hs Code.:

C<sub>39</sub>H<sub>45</sub>NO<sub>3</sub>S<sub>3</sub>Si

Synonyms:C₃₉H₄₅NO₃S₃Si

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Chemical Property of C₃₉H₄₅NO₃S₃Si

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Technology Process of C₃₉H₄₅NO₃S₃Si

There total 5 articles about C₃₉H₄₅NO₃S₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1261033-30-0
C₂₇H₃₅NO₄SSi

: 108-98-5
thiophenol

: 1261033-32-2
C₃₉H₄₅NO₃S₃Si

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201001402

Reference yield:

: 1261034-19-8
C₂₇H₃₃NO₄SSi

: 1261033-32-2
C₃₉H₄₅NO₃S₃Si

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hexamethylsilazane / -100 °C / Inert atmosphere

2: 10% palladium on activated carbon; hydrogen / ethanol / 760.05 Torr / Inert atmosphere

3: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

With 10% palladium on activated carbon; boron trifluoride diethyl etherate; hydrogen; potassium hexamethylsilazane; In ethanol; dichloromethane; 1: Michael cyclization;
DOI:10.1002/chem.201001402

Reference yield:

: 1261033-27-5
C₂₇H₃₃NO₄SSi

: 1261033-32-2
C₃₉H₄₅NO₃S₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: 10% palladium on activated carbon; hydrogen / ethanol / 760.05 Torr / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

With 10% palladium on activated carbon; boron trifluoride diethyl etherate; hydrogen; In ethanol; dichloromethane;
DOI:10.1002/chem.201001402