1-[2-(4-chlorophenyl)ethyl]-3-[(3,4-dihydroxyphenyl)methyl]-3-methylthiourea

Base Information

Chemical Name:1-[2-(4-chlorophenyl)ethyl]-3-[(3,4-dihydroxyphenyl)methyl]-3-methylthiourea
CAS No.:1025423-97-5
Molecular Formula:C₁₇H₁₉ClN₂O₂S
Molecular Weight:350.869
Hs Code.:

Synonyms:1-[2-(4-chlorophenyl)ethyl]-3-[(3,4-dihydroxyphenyl)methyl]-3-methylthiourea

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[2-(4-chlorophenyl)ethyl]-3-[(3,4-dihydroxyphenyl)methyl]-3-methylthiourea

Chemical Property:

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Technology Process of 1-[2-(4-chlorophenyl)ethyl]-3-[(3,4-dihydroxyphenyl)methyl]-3-methylthiourea

There total 3 articles about 1-[2-(4-chlorophenyl)ethyl]-3-[(3,4-dihydroxyphenyl)methyl]-3-methylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1025423-95-3
4-[(methylamino)methyl]benzene-1,2-diol hydrobromide

: 17608-10-5
2-(4-chlorophenyl)ethyl isothiocyanate

: 1025423-97-5
1-[2-(4-chlorophenyl)ethyl]-3-[(3,4-dihydroxyphenyl)methyl]-3-methylthiourea

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1016/j.bmc.2007.11.055

Reference yield:

: 17608-10-5
2-(4-chlorophenyl)ethyl isothiocyanate

: 125789-62-0
4-methylaminomethyl-pyrocatechol

: 1025423-97-5
1-[2-(4-chlorophenyl)ethyl]-3-[(3,4-dihydroxyphenyl)methyl]-3-methylthiourea

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2018.11.040

Reference yield:

: 156-41-2
4-chlorophenylethylamine

: 1025423-97-5
1-[2-(4-chlorophenyl)ethyl]-3-[(3,4-dihydroxyphenyl)methyl]-3-methylthiourea

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 20 °C

With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2018.11.040