syn-7-Bromomethylsulfonyl-exo-6-hydroxy-endo-6-phenylbicyclo[3.1.1]heptane

Base Information

Chemical Name:syn-7-Bromomethylsulfonyl-exo-6-hydroxy-endo-6-phenylbicyclo[3.1.1]heptane
CAS No.:271252-51-8
Molecular Formula:C₁₄H₁₇BrO₃S
Molecular Weight:345.257
Hs Code.:

Synonyms:syn-7-Bromomethylsulfonyl-exo-6-hydroxy-endo-6-phenylbicyclo[3.1.1]heptane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of syn-7-Bromomethylsulfonyl-exo-6-hydroxy-endo-6-phenylbicyclo[3.1.1]heptane

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Technology Process of syn-7-Bromomethylsulfonyl-exo-6-hydroxy-endo-6-phenylbicyclo[3.1.1]heptane

There total 3 articles about syn-7-Bromomethylsulfonyl-exo-6-hydroxy-endo-6-phenylbicyclo[3.1.1]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 7-syn-bromomethylsulfonyl-6-endo-phenylbicyclo[3.1.1]hept-6-exo-yl thiocyanate

: 271252-51-8
syn-7-Bromomethylsulfonyl-exo-6-hydroxy-endo-6-phenylbicyclo[3.1.1]heptane

Guidance literature:: With water; silver nitrate; In 1,4-dioxane; at 20 ℃; Darkness;
DOI:10.1134/S1070428012040057

Reference yield: 78.0%

: 271252-15-4
exo-6-Bromo-syn-7-bromomethylsulfonyl-endo-6-phenylbicyclo[3.1.1]heptane

: 271252-51-8
syn-7-Bromomethylsulfonyl-exo-6-hydroxy-endo-6-phenylbicyclo[3.1.1]heptane

Guidance literature:: With water; sodium carbonate; In tetrahydrofuran; for 1h; Heating;

Reference yield:

: 57293-39-7
1-Phenyltricyclo<4.1.0.0.^2,7>heptane

: 271252-51-8
syn-7-Bromomethylsulfonyl-exo-6-hydroxy-endo-6-phenylbicyclo[3.1.1]heptane

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / CaCO₃ / CH₂Cl₂ / 14 h / 0 °C

2: 78 percent / Na₂CO₃; H₂O / tetrahydrofuran / 1 h / Heating

With water; sodium carbonate; calcium carbonate; In tetrahydrofuran; dichloromethane; 1: Addition / 2: Hydrolysis;