N-(4-bromophenyl)-2-(7-bromo-9,9-diethylfluoren-2-yl)isoindole-1-carboxamide

Base Information

Chemical Name:N-(4-bromophenyl)-2-(7-bromo-9,9-diethylfluoren-2-yl)isoindole-1-carboxamide
CAS No.:1608155-12-9
Molecular Formula:C₃₂H₂₆Br₂N₂O
Molecular Weight:614.379
Hs Code.:

Synonyms:N-(4-bromophenyl)-2-(7-bromo-9,9-diethylfluoren-2-yl)isoindole-1-carboxamide

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Chemical Property of N-(4-bromophenyl)-2-(7-bromo-9,9-diethylfluoren-2-yl)isoindole-1-carboxamide

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Technology Process of N-(4-bromophenyl)-2-(7-bromo-9,9-diethylfluoren-2-yl)isoindole-1-carboxamide

There total 3 articles about N-(4-bromophenyl)-2-(7-bromo-9,9-diethylfluoren-2-yl)isoindole-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1202709-54-3
7-bromo-9,9-diethyl-9H-fluoren-2-amine

: 33554-73-3
1-bromo-4-isocyanobenzene

: 643-79-8
o-phthalic dicarboxaldehyde

: 1608155-12-9
N-(4-bromophenyl)-2-(7-bromo-9,9-diethylfluoren-2-yl)isoindole-1-carboxamide

Guidance literature:: o-phthalic dicarboxaldehyde; With sodium hydrogen sulfate; In water; dimethyl sulfoxide; at 20 ℃; for 0.5h; Darkness; Inert atmosphere;

7-bromo-9,9-diethyl-9H-fluoren-2-amine; 1-bromo-4-isocyanobenzene; In water; dimethyl sulfoxide; acetonitrile; at 20 - 100 ℃; for 4h; Darkness; Inert atmosphere;
DOI:10.1016/j.tet.2014.04.018

Reference yield:

: 2-bromo-7-nitro-9,9-diethylfluorene

: 1608155-12-9
N-(4-bromophenyl)-2-(7-bromo-9,9-diethylfluoren-2-yl)isoindole-1-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: iron; ammonium chloride / ethanol; water / 2 h / 85 °C / Reflux; Inert atmosphere

2.1: sodium hydrogen sulfate / water; dimethyl sulfoxide / 0.5 h / 20 °C / Darkness; Inert atmosphere

2.2: 4 h / 20 - 100 °C / Darkness; Inert atmosphere

With sodium hydrogen sulfate; iron; ammonium chloride; In ethanol; water; dimethyl sulfoxide;
DOI:10.1016/j.tet.2014.04.018

Reference yield:

: 287493-15-6
2-bromo-9,9-diethyl-9H-fluorene

: 1608155-12-9
N-(4-bromophenyl)-2-(7-bromo-9,9-diethylfluoren-2-yl)isoindole-1-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: nitric acid / dichloromethane / 0.17 h / 20 °C

2.1: iron; ammonium chloride / ethanol; water / 2 h / 85 °C / Reflux; Inert atmosphere

3.1: sodium hydrogen sulfate / water; dimethyl sulfoxide / 0.5 h / 20 °C / Darkness; Inert atmosphere

3.2: 4 h / 20 - 100 °C / Darkness; Inert atmosphere

With sodium hydrogen sulfate; nitric acid; iron; ammonium chloride; In ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/j.tet.2014.04.018