(2S,3S)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate

Base Information

Chemical Name:(2S,3S)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate
CAS No.:1403165-05-8
Molecular Formula:C₂₉H₂₅N₃O₆S
Molecular Weight:543.6
Hs Code.:

Synonyms:(2S,3S)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate

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Chemical Property of (2S,3S)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate

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Technology Process of (2S,3S)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate

There total 2 articles about (2S,3S)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63160-16-7
4-nitro-N-(phenylmethylene)benzenesulfonamide

: 81167-39-7
methyl N-(diphenylmethylene)glycinate

: 1403164-71-5
(2S,3R)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate

: 1403165-05-8
(2S,3S)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate

Guidance literature:: With 2,6-bis((2R,4S,5S)-1-benzyl-4,5-diphenylimidazolidin-2-yl)pyridine; copper(II) bis(trifluoromethanesulfonate); N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 ℃; for 36h; Overall yield = 90 %; stereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.201201537

Reference yield:

: 63160-16-7
4-nitro-N-(phenylmethylene)benzenesulfonamide

: 81167-39-7
methyl N-(diphenylmethylene)glycinate

: 1403164-71-5
(2S,3R)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate

: 1403165-05-8
(2S,3S)-methyl 2-(diphenylmethyleneamino)-3-(4-nitrophenylsulfonamido)-3-phenylpropanoate

: C₂₉H₂₅N₃O₆S

: C₂₉H₂₅N₃O₆S

Guidance literature:: With silver trifluoromethanesulfonate; (3,5-Dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-((R)-1-phenyl-ethyl)-amine; In toluene; at 20 ℃; Overall yield = 100 %Spectr.; enantioselective reaction;
DOI:10.1016/j.tetasy.2014.11.009