C₃₉H₅₅ClN₁₀O₄

Base Information

Chemical Name:C₃₉H₅₅ClN₁₀O₄
CAS No.:1613708-30-7
Molecular Formula:C₃₉H₅₅ClN₁₀O₄
Molecular Weight:763.383
Hs Code.:

C<sub>39</sub>H<sub>55</sub>ClN<sub>10</sub>O<sub>4</sub>

Synonyms:C₃₉H₅₅ClN₁₀O₄

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Chemical Property of C₃₉H₅₅ClN₁₀O₄

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Technology Process of C₃₉H₅₅ClN₁₀O₄

There total 22 articles about C₃₉H₅₅ClN₁₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 76942-92-2
methyl 3,5-diamino-6-chloropyrazine-2-carbonylcarbamimidothioate hydroiodic acid salt

: 1613708-29-4
C₃₃H₅₀N₄O₃*C₂H₄O₂

: 1613708-30-7
C₃₉H₅₅ClN₁₀O₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; at 70 ℃; for 2h; Sealed tube;

Reference yield:

: 42817-60-7
N-[3-(4-aminophenyl)propyl]-N,N-dimethylamine

: 1613708-30-7
C₃₉H₅₅ClN₁₀O₄

Guidance literature:: Multi-step reaction with 3 steps

1: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 12 h / 20 °C / 760.05 Torr

3: N-ethyl-N,N-diisopropylamine / ethanol / 2 h / 70 °C / Sealed tube

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; ethanol;

Reference yield:

: 529-35-1
5,6,7,8-Tetrahydronaphthalen-1-ol

: 1613708-30-7
C₃₉H₅₅ClN₁₀O₄

Guidance literature:: Multi-step reaction with 18 steps

1.1: sodium hydroxide / 2 h / 0 - 20 °C

2.1: trichlorophosphate / dichloromethane / 6 h / 0 - 80 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / 0 °C

3.2: 16 h / 20 °C

4.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / 760.05 Torr

5.1: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

6.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 1.5 h / -78 - -20 °C

6.2: 1.67 h / -78 - 20 °C

7.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

7.2: 0.08 h

7.3: 16 h / 24 °C

8.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.17 h / 0 - 20 °C

9.1: palladium 10% on activated carbon; hydrogen; acetic acid / water / 3 h / 20 °C / 760.05 Torr

10.1: acetic acid; hydrogen bromide / 3 h / Reflux

11.1: acetyl chloride / 4 h / 0 °C / Reflux

12.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C

13.1: pyridine / dichloromethane / 3 h / 0 - 20 °C

14.1: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

15.1: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

16.1: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

17.1: palladium 10% on activated carbon; hydrogen / ethanol / 12 h / 20 °C / 760.05 Torr

18.1: N-ethyl-N,N-diisopropylamine / ethanol / 2 h / 70 °C / Sealed tube

With 4-methyl-morpholine; pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; lithium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetonitrile;