O-(2,3:4,5-di-O-isopropylidene-β-D-glucoseptanosyl) trichloroacetimidate

Base Information

Chemical Name:O-(2,3:4,5-di-O-isopropylidene-β-D-glucoseptanosyl) trichloroacetimidate
CAS No.:1379587-24-2
Molecular Formula:C₁₄H₂₀Cl₃NO₆
Molecular Weight:404.675
Hs Code.:

Synonyms:O-(2,3:4,5-di-O-isopropylidene-β-D-glucoseptanosyl) trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(2,3:4,5-di-O-isopropylidene-β-D-glucoseptanosyl) trichloroacetimidate

Chemical Property:

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Technology Process of O-(2,3:4,5-di-O-isopropylidene-β-D-glucoseptanosyl) trichloroacetimidate

There total 1 articles about O-(2,3:4,5-di-O-isopropylidene-β-D-glucoseptanosyl) trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.5%

: 1379587-23-1
ethyl 1-thio-2,3:4,5-di-O-isopropylidene-α-D-glucoseptanoside

: 1379587-25-3
ethyl 1-thio-α-D-glucoseptanoside

: 1379587-24-2
O-(2,3:4,5-di-O-isopropylidene-β-D-glucoseptanosyl) trichloroacetimidate

: 7473-36-1,13533-58-9,36400-88-1,56245-60-4,73494-52-7,73804-33-8,128946-17-8,686299-00-3
(2R,3R,4S,5S,6R)-2-Ethylsulfanyl-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With hydrogenchloride; water; In ethanol; at 40 ℃; for 70h;
DOI:10.1016/j.carres.2012.03.011

Reference yield:

: 1379587-24-2
O-(2,3:4,5-di-O-isopropylidene-β-D-glucoseptanosyl) trichloroacetimidate

: 1379587-26-4
ethyl 1-thio-2,3,4,5-tetra-O-acetyl-α-D-glucoseptanoside

: 32934-24-0,41670-79-5,52645-73-5,55722-49-1,79389-52-9,99031-86-4,125354-48-5,126187-25-5
ethyl 2,3,4,6-tetra-O-acetyl-1-thio-α-D-glycopyranoside

: 39697-82-0,98975-54-3
ethyl 1-thio-α-D-glucofuranoside tetraacetate

Guidance literature:: Multi-step reaction with 2 steps

1: zinc(II) chloride / dichloromethane / 25 h / Molecular sieve

2: hydrogenchloride; water / ethanol / 70 h / 40 °C

With hydrogenchloride; water; zinc(II) chloride; In ethanol; dichloromethane;
DOI:10.1016/j.carres.2012.03.011

Reference yield:

: 1379587-24-2
O-(2,3:4,5-di-O-isopropylidene-β-D-glucoseptanosyl) trichloroacetimidate

: 1379587-25-3
ethyl 1-thio-α-D-glucoseptanoside

: 7473-36-1,13533-58-9,36400-88-1,56245-60-4,73494-52-7,73804-33-8,128946-17-8,686299-00-3
(2R,3R,4S,5S,6R)-2-Ethylsulfanyl-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 2 steps

1: zinc(II) chloride / dichloromethane / 25 h / Molecular sieve

2: hydrogenchloride; water / ethanol / 70 h / 40 °C

With hydrogenchloride; water; zinc(II) chloride; In ethanol; dichloromethane;
DOI:10.1016/j.carres.2012.03.011