3-(2,4,6-trimethyl-phenyl)-(3ar,8bc)-3a,8b-dihydro-benzo[4,5]thieno[2,3-d]isoxazole

Base Information

• Chemical Name: 3-(2,4,6-trimethyl-phenyl)-(3ar,8bc)-3a,8b-dihydro-benzo[4,5]thieno[2,3-d]isoxazole
• CAS No.: 70608-20-7
• Molecular Formula: C₁₈H₁₇NOS
• Molecular Weight: 295.405

Synonyms:3-(2,4,6-trimethyl-phenyl)-(3ar,8bc)-3a,8b-dihydro-benzo[4,5]thieno[2,3-d]isoxazole

Chemical Property of 3-(2,4,6-trimethyl-phenyl)-(3ar,8bc)-3a,8b-dihydro-benzo[4,5]thieno[2,3-d]isoxazole

Chemical Property:

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Technology Process of 3-(2,4,6-trimethyl-phenyl)-(3ar,8bc)-3a,8b-dihydro-benzo[4,5]thieno[2,3-d]isoxazole

There total 1 articles about 3-(2,4,6-trimethyl-phenyl)-(3ar,8bc)-3a,8b-dihydro-benzo[4,5]thieno[2,3-d]isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

mesitylenecarbonitrile oxide (2904-57-6) + Benzo[b]thiophene (95-15-8,11095-43-5) → 3-(2,4,6-trimethyl-phenyl)-(3ar,8bc)-3a,8b-dihydro-benzo[4,5]thieno[2,3-d]isoxazole (70608-20-7)

Guidance literature:

In benzene;

DOI:10.1016/0040-4020(78)88430-0

Reference yield: 80.0%

3-(2,4,6-trimethyl-phenyl)-(3ar,8bc)-3a,8b-dihydro-benzo[4,5]thieno[2,3-d]isoxazole (70608-20-7) → 4,4-dioxo-3-(2,4,6-trimethylphenyl)-2,3-dihydrobenzothiopheno<2,3-d>isoxazoline (86559-01-5)

Guidance literature:

With dihydrogen peroxide; In acetic acid; for 1h; Heating;

DOI:10.1016/0040-4020(82)80071-9

upstream raw materials:

mesitylenecarbonitrile oxide

Benzo[b]thiophene

Downstream raw materials:

4,4-dioxo-3-(2,4,6-trimethylphenyl)-2,3-dihydrobenzothiopheno<2,3-d>isoxazoline

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