5-((4-chlorophenyl)sulfonylmethylene)-3-(2,2,2-trifluoroethyl)-5H-furan-2-one

Base Information

• Chemical Name: 5-((4-chlorophenyl)sulfonylmethylene)-3-(2,2,2-trifluoroethyl)-5H-furan-2-one
• CAS No.: 1392267-40-1
• Molecular Formula: C₁₃H₈ClF₃O₄S
• Molecular Weight: 352.718

Synonyms:5-((4-chlorophenyl)sulfonylmethylene)-3-(2,2,2-trifluoroethyl)-5H-furan-2-one

Chemical Property of 5-((4-chlorophenyl)sulfonylmethylene)-3-(2,2,2-trifluoroethyl)-5H-furan-2-one

Chemical Property:

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Technology Process of 5-((4-chlorophenyl)sulfonylmethylene)-3-(2,2,2-trifluoroethyl)-5H-furan-2-one

There total 2 articles about 5-((4-chlorophenyl)sulfonylmethylene)-3-(2,2,2-trifluoroethyl)-5H-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C13H8ClF3O2S (889110-29-6) → 5-((4-chlorophenyl)sulfonylmethylene)-3-(2,2,2-trifluoroethyl)-5H-furan-2-one (1392267-40-1)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1021/jm301076q

Reference yield:

4-oxo-2-pentafluoroethyl-pentanethioic acid S-(4-chloro-phenyl) ester (889110-27-4) → 5-((4-chlorophenyl)sulfonylmethylene)-3-(2,2,2-trifluoroethyl)-5H-furan-2-one (1392267-40-1)

Guidance literature:

Multi-step reaction with 2 steps

1: diisopropylamine / diethyl ether / 15 h / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 20 °C

With diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;

DOI:10.1021/jm301076q

Reference yield: 36.0%

5-((4-chlorophenyl)sulfonylmethylene)-3-(2,2,2-trifluoroethyl)-5H-furan-2-one (1392267-40-1) + N1-(7-chloroquinolin-4-yl)butane-1,4-diamine (53186-45-1) → C26H24Cl2F3N3O4S (1392267-05-8)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1021/jm301076q

upstream raw materials:

4-oxo-2-pentafluoroethyl-pentanethioic acid S-(4-chloro-phenyl) ester

C₁₃H₈ClF₃O₂S

Downstream raw materials:

C₂₆H₂₄Cl₂F₃N₃O₄S

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