10-phenyl-3,4-dihydro-2H,10aH-1-oxa-4a,9-diazaphenanthrene

Base Information

Chemical Name:10-phenyl-3,4-dihydro-2H,10aH-1-oxa-4a,9-diazaphenanthrene
CAS No.:1634721-95-1
Molecular Formula:C₁₇H₁₆N₂O
Molecular Weight:264.327
Hs Code.:

Synonyms:10-phenyl-3,4-dihydro-2H,10aH-1-oxa-4a,9-diazaphenanthrene

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Chemical Property of 10-phenyl-3,4-dihydro-2H,10aH-1-oxa-4a,9-diazaphenanthrene

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Technology Process of 10-phenyl-3,4-dihydro-2H,10aH-1-oxa-4a,9-diazaphenanthrene

There total 5 articles about 10-phenyl-3,4-dihydro-2H,10aH-1-oxa-4a,9-diazaphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1057226-65-9
3-[(3-phenyl)-2-oxo-2H-quinoxalin-1-yl]propionic acid ethyl ester

: 1634721-95-1
10-phenyl-3,4-dihydro-2H,10aH-1-oxa-4a,9-diazaphenanthrene

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 10 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.14233/ajchem.2014.15859

Reference yield:

: 23465-73-8
3-Phenyl-1,2,3,4-tetrahydroquinoxalin-2-one

: 1634721-95-1
10-phenyl-3,4-dihydro-2H,10aH-1-oxa-4a,9-diazaphenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 20 °C / Inert atmosphere; Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 10 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.14233/ajchem.2014.15859

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1634721-95-1
10-phenyl-3,4-dihydro-2H,10aH-1-oxa-4a,9-diazaphenanthrene

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 60 °C / Inert atmosphere

2: toluene-4-sulfonic acid / toluene / 20 °C / Inert atmosphere; Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 10 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.14233/ajchem.2014.15859