N₄,N₈-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-(2,3-dimethoxybenzoyl)thermospermine

Base Information

• Chemical Name: N₄,N₈-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-(2,3-dimethoxybenzoyl)thermospermine
• CAS No.: 1154500-27-2
• Molecular Formula: C₃₇H₆₄N₆O₁₁
• Molecular Weight: 768.949

Synonyms:N₄,N₈-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-(2,3-dimethoxybenzoyl)thermospermine

Chemical Property of N₄,N₈-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-(2,3-dimethoxybenzoyl)thermospermine

Chemical Property:

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Technology Process of N₄,N₈-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-(2,3-dimethoxybenzoyl)thermospermine

There total 1 articles about N₄,N₈-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-(2,3-dimethoxybenzoyl)thermospermine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

N4,N7-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N1-(2,3-dimethoxybenzoyl)-N7-[4-(phthalimido)butyl]norspermidine (1154500-25-0) → N4,N8-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N1-(2,3-dimethoxybenzoyl)thermospermine (1154500-27-2)

Guidance literature:

With hydrazine hydrate; In ethanol; at 20 ℃; for 16h;

DOI:10.1021/jm900119q

Reference yield: 40.0%

3,3'-dithiobis(propionic acid) (1119-62-6) + N4,N8-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N1-(2,3-dimethoxybenzoyl)thermospermine (1154500-27-2) → 1,36-bis(2,3-dimethoxybenzoyl)-15,22-dioxo-18,19-dithia-1,5,9,14,23,28,32,36-octaaza-5,9,28,32-tetrakis[(N-tert-butoxycarbonyl)-L-threonyl]hexatriacontane (1154500-29-4)

Guidance literature:

3,3'-dithiobis(propionic acid); With 1,1'-carbonyldiimidazole; In dichloromethane; for 2h;

N₄,N₈-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-(2,3-dimethoxybenzoyl)thermospermine; In dichloromethane; at 20 ℃; for 15h;

DOI:10.1021/jm900119q

upstream raw materials:

N₄,N₇-bis[(N-tert-butoxycarbonyl)-L-threonyl]-N₁-(2,3-dimethoxybenzoyl)-N₇-[4-(phthalimido)butyl]norspermidine

Downstream raw materials:

1,36-bis(2,3-dimethoxybenzoyl)-15,22-dioxo-18,19-dithia-1,5,9,14,23,28,32,36-octaaza-5,9,28,32-tetrakis[(N-tert-butoxycarbonyl)-L-threonyl]hexatriacontane

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