[Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2PF₆^(1-)*(CH₃)2CO=[Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](PF₆)2*(CH₃)2CO

Base Information

• Chemical Name: [Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2PF₆^(1-)*(CH₃)2CO=[Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](PF₆)2*(CH₃)2CO
• CAS No.: 86992-66-7
• Molecular Formula: C₃H₆O*C₆₂H₅₀N₂O₂P₄Rh₂*2F₆P
• Molecular Weight: 1532.81

Synonyms:[Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2PF₆^(1-)*(CH₃)2CO=[Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](PF₆)2*(CH₃)2CO

Chemical Property of [Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2PF₆^(1-)*(CH₃)2CO=[Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](PF₆)2*(CH₃)2CO

Chemical Property:

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Technology Process of [Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2PF₆^(1-)*(CH₃)2CO=[Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](PF₆)2*(CH₃)2CO

There total 1 articles about [Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2PF₆^(1-)*(CH₃)2CO=[Rh₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](PF₆)2*(CH₃)2CO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Rh(CO)(Cl)(((C6H5)2P)2CHC5H4N) (86943-74-0) → [Rh2(CO)2(((C6H5)2P)2CHC5H4N)2](2+) (86992-66-7)

Guidance literature:

In water; acetone; under N2, addn. of water (only 5% by vol.) to acetone soln. of educt; detected spectroscopically;

Reference yield: 75.0%

[Rh2(CO)2(((C6H5)2P)2CHC5H4N)2](2+)*2PF6(1-)*(CH3)2CO=[Rh2(CO)2(((C6H5)2P)2CHC5H4N)2](PF6)2*(CH3)2CO (86992-66-7) → Rh2(S)(CO)2(((C6H5)2P)2CHC5H4N)2 (86943-73-9)

Guidance literature:

With sodium sulfide; In methanol; under N2, dry Na2S dissolved in dry methanol added to slurry of Rh complex in methanol, stirred for 1 h; ppt. collected by filtration, washed with dry methanol, crystd. from acetone/hexane; elem. anal.;

Reference yield: 38.0%

[Rh2(CO)2(((C6H5)2P)2CHC5H4N)2](2+)*2PF6(1-)*(CH3)2CO=[Rh2(CO)2(((C6H5)2P)2CHC5H4N)2](PF6)2*(CH3)2CO (86992-66-7) + tetraethylammonium chloride monohydrate (68696-18-4) → Rh(CO)(Cl)(((C6H5)2P)2CHC5H4N) (86943-74-0)

Guidance literature:

In acetone; under N2, Rh complex disoolved in dry acetone, satd. acetone soln. of NEt4Cl*H2O added dropwise; dried over anhyd. Na2SO4 for 1 h, filtered, cooled to -78°C, layered with hexane, allowed to stand at room temp. for 24 h, solvents syringed off, solids dried in stream of N2, crystals sepd. manually; elem. anal.;

upstream raw materials:

Rh(CO)(Cl)(((C₆H₅)2P)2CHC₅H₄N)

Downstream raw materials:

Rh₂(S)(CO)2(((C₆H₅)2P)2CHC₅H₄N)2

Rh(CO)(Cl)(((C₆H₅)2P)2CHC₅H₄N)

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