phenyl (7S)-N'-cyano-N-(7-(t-butoxycarbonylamino)-6,7,8,9-tetrahydro-5H-benzo[7]annulene-2-yl)carbamimidate

Base Information

Chemical Name:phenyl (7S)-N'-cyano-N-(7-(t-butoxycarbonylamino)-6,7,8,9-tetrahydro-5H-benzo[7]annulene-2-yl)carbamimidate
CAS No.:1204249-43-3
Molecular Formula:C₂₄H₂₈N₄O₃
Molecular Weight:420.511
Hs Code.:

Synonyms:phenyl (7S)-N'-cyano-N-(7-(t-butoxycarbonylamino)-6,7,8,9-tetrahydro-5H-benzo[7]annulene-2-yl)carbamimidate

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Chemical Property of phenyl (7S)-N'-cyano-N-(7-(t-butoxycarbonylamino)-6,7,8,9-tetrahydro-5H-benzo[7]annulene-2-yl)carbamimidate

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Technology Process of phenyl (7S)-N'-cyano-N-(7-(t-butoxycarbonylamino)-6,7,8,9-tetrahydro-5H-benzo[7]annulene-2-yl)carbamimidate

There total 6 articles about phenyl (7S)-N'-cyano-N-(7-(t-butoxycarbonylamino)-6,7,8,9-tetrahydro-5H-benzo[7]annulene-2-yl)carbamimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₄N₂O₂

: 79463-77-7
N-cyanodiphenylcarbonimidate

: 1204249-43-3
phenyl (7S)-N'-cyano-N-(7-(t-butoxycarbonylamino)-6,7,8,9-tetrahydro-5H-benzo[7]annulene-2-yl)carbamimidate

Guidance literature:: In isopropyl alcohol; at 20 ℃;

Reference yield:

: 168893-82-1
diphenyl cyanocarbonimidate

: C₁₆H₂₄N₂O₂

: 1204249-43-3
phenyl (7S)-N'-cyano-N-(7-(t-butoxycarbonylamino)-6,7,8,9-tetrahydro-5H-benzo[7]annulene-2-yl)carbamimidate

Guidance literature:: In isopropyl alcohol; at 20 ℃;

Reference yield:

: 24790-66-7
dimethyl 1,2,4,5-tetrahydro-3-oxobenzocycloheptene-2,4-dicarboxylate

: 1204249-43-3
phenyl (7S)-N'-cyano-N-(7-(t-butoxycarbonylamino)-6,7,8,9-tetrahydro-5H-benzo[7]annulene-2-yl)carbamimidate

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; potassium hydroxide / ethanol / 17 h / 85 °C

2.1: nitric acid; sulfuric acid / nitromethane / 2.67 h / 0 °C

3.1: L-alanin / aq. buffer / 0.33 h

3.2: The pyruvate reductase mix; the transaminase / 144 h / pH 7 - 7.5

5.1: isopropyl alcohol / 20 °C

With L-alanin; sulfuric acid; water; nitric acid; potassium hydroxide; In nitromethane; ethanol; isopropyl alcohol;