Technology Process of C40H48N6O9
There total 8 articles about C40H48N6O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/ja412729s
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium hydroxide / 1,4-dioxane; water / 16 h / 20 °C / Inert atmosphere
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
3: dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere
4: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 72 h / 80 °C / Inert atmosphere
5: trifluoroacetic acid / dichloromethane / 4 h / 20 °C / Inert atmosphere
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; potassium hydroxide;
In
1,4-dioxane; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja412729s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
2: dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 72 h / 80 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane / 4 h / 20 °C / Inert atmosphere
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja412729s