C₁₇H₁₈O₂

Base Information

• Chemical Name: C₁₇H₁₈O₂
• CAS No.: 1319203-97-8
• Molecular Formula: C₁₇H₁₈O₂
• Molecular Weight: 254.329
• Mol file: 1319203-97-8.mol

Synonyms:C₁₇H₁₈O₂

Chemical Property of C₁₇H₁₈O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₈O₂

There total 8 articles about C₁₇H₁₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

C23H32O2Si (1319203-99-0) → C17H18O2 (1319203-97-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c1ob05725a

Reference yield:

2-vinylbenzoic acid (27326-43-8) → C17H18O2 (1319203-97-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere

2.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

2.2: 0.42 h / 0 °C / Inert atmosphere

3.1: magnesium; ethylene dibromide / diethyl ether / 2 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; magnesium; ethylene dibromide; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1039/c1ob05725a

Reference yield:

o-carboxybenzaldehyde (119-67-5) → C17H18O2 (1319203-97-8)

Guidance literature:

Multi-step reaction with 5 steps

1.1: potassium tert-butylate / tetrahydrofuran / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere

3.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

3.2: 0.42 h / 0 °C / Inert atmosphere

4.1: magnesium; ethylene dibromide / diethyl ether / 2 h / 20 °C / Inert atmosphere

4.2: 1 h / 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium tert-butylate; tetrabutyl ammonium fluoride; magnesium; ethylene dibromide; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; 1.1: Wittig olefination;

DOI:10.1039/c1ob05725a

upstream raw materials:

C₂₃H₃₂O₂Si

2-vinylbenzoic acid

2-vinylbenzylalcohol

vinylbenzyl bromide