4,4-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1-terphenyl-3,3-diol

Base Information

Chemical Name:4,4-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1-terphenyl-3,3-diol
CAS No.:1075724-39-8
Molecular Formula:C₃₀H₃₄O₈
Molecular Weight:522.595
Hs Code.:

Synonyms:4,4-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1-terphenyl-3,3-diol

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Chemical Property of 4,4-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1-terphenyl-3,3-diol

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Technology Process of 4,4-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1-terphenyl-3,3-diol

There total 1 articles about 4,4-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1-terphenyl-3,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 3,3''-benzyloxy-4,4''-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1''-terphenyl

: 1075724-39-8
4,4-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1-terphenyl-3,3-diol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 45 ℃; for 6h; under 2400.24 Torr;
DOI:10.1021/ja110065r

Reference yield: 81.0%

: 1075724-39-8
4,4-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1-terphenyl-3,3-diol

: 1282043-33-7
16-bromomethyl-1,1,1,2,2,3,3,4,4,28,28,29,29,30,30,31,31,31-octadecafluorohentriacontane

: 4,4''-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-3,3''-bis[2,2-bis(12,12,13,13,14,14,15,15,15-nonafluoropentadecyl)ethoxy]-1,1':4',1''-terphenyl

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 6h;
DOI:10.1021/ja110065r

Reference yield: 64.0%

: 1075724-39-8
4,4-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-1,1':4',1-terphenyl-3,3-diol

: 1282043-27-9
8-bromomethyl-1,1,1,2,2,3,3,4,4-nonafluoropentadecane

: 1282043-36-0
4,4''-bis(2,2-dimethyl-1,3-dioxolan-4-ylmethoxy)-3,3''-bis(6,6,7,7,8,8,9,9,9-nonafluoro-2-heptylnonyloxy)-1,1':4',1''-terphenyl

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 6h;
DOI:10.1021/ja110065r