[((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-)

Base Information

• Chemical Name: [((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-)
• CAS No.: 258519-05-0
• Molecular Formula: C₁₉H₃BF₁₅*C₂₅H₅₅Al₂N₄
• Molecular Weight: 992.721

Synonyms:[((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-)

Chemical Property of [((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-)

Chemical Property:

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Technology Process of [((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-)

There total 2 articles about [((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*[CH₃B(C₆F₅)3]^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

((t)BuC(N(isopropyl))2)AlMe2 (194655-52-2) + tris(pentafluorophenyl)borate (1109-15-5) → [((CH3)3CC(NCH(CH3)2)2)Al(CH3)2((CH3)3CC(NCH(CH3)2)2)AlCH3](1+)*[CH3B(C6F5)3](1-) (258519-05-0)

Guidance literature:

In dichloromethane-d2; in sealed tube, mixing at -78°C, then 20 min at -60°C; not isolated; NMR;

DOI:10.1021/ja992104j

Reference yield:

[((CH3)3CC(NCH(CH3)2)2)Al(CH3)2((CH3)3CC(NCH(CH3)2)2)AlCH3](1+)*B(C6F5)4(1-) (258519-01-6) → [((CH3)3CC(NCH(CH3)2)2)Al(CH3)2((CH3)3CC(NCH(CH3)2)2)AlCH3](1+)*[CH3B(C6F5)3](1-) (258519-05-0)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane-d2

2: dichloromethane-d2

In dichloromethane-d2;

DOI:10.1021/ja992104j

Reference yield:

[((CH3)3CC(NCH(CH3)2)2)Al(CH3)2((CH3)3CC(NCH(CH3)2)2)AlCH3](1+)*[CH3B(C6F5)3](1-) (258519-05-0) → ((CH3)3CC(NCH(CH3)2)2)Al(CH3)(C6F5) (258519-16-3) + methylbis(pentafluorophenyl)borane (170151-48-1)

Guidance literature:

In dichloromethane-d2; in sealed tube; warming above 0°C; not isolated; NMR;

DOI:10.1021/ja992104j

upstream raw materials:

((t)BuC(N(isopropyl))2)AlMe₂

tris(pentafluorophenyl)borate

[((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)2((CH₃)3CC(NCH(CH₃)2)2)AlCH₃]⁽¹⁺⁾*B(C₆F₅)4^(1-)

Downstream raw materials:

((CH₃)3CC(NCH(CH₃)2)2)Al(CH₃)(C₆F₅)

methylbis(pentafluorophenyl)borane

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