2H-Furo[3,2-b]pyrrol-2-ol, 4-acetylhexahydro-, [2R-(2alpha,3abeta,6abeta)]- (9CI)

Base Information

Chemical Name:2H-Furo[3,2-b]pyrrol-2-ol, 4-acetylhexahydro-, [2R-(2alpha,3abeta,6abeta)]- (9CI)
CAS No.:115996-13-9
Molecular Formula:C₈H₁₃NO₃
Molecular Weight:171.196
Hs Code.:
Mol file:115996-13-9.mol

Synonyms:2H-Furo[3,2-b]pyrrol-2-ol, 4-acetylhexahydro-, [2R-(2alpha,3abeta,6abeta)]- (9CI)

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Chemical Property of 2H-Furo[3,2-b]pyrrol-2-ol, 4-acetylhexahydro-, [2R-(2alpha,3abeta,6abeta)]- (9CI)

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Technology Process of 2H-Furo[3,2-b]pyrrol-2-ol, 4-acetylhexahydro-, [2R-(2alpha,3abeta,6abeta)]- (9CI)

There total 15 articles about 2H-Furo[3,2-b]pyrrol-2-ol, 4-acetylhexahydro-, [2R-(2alpha,3abeta,6abeta)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 107690-64-2,116050-85-2
methyl 3,6-acetylepimino-2,3,5,6-tetradeoxy-(α,β)-D-threo-hexofuranoside

: 115996-13-9,116050-86-3
1-((3aR,6aR)-2-Hydroxy-hexahydro-furo[3,2-b]pyrrol-4-yl)-ethanone

Guidance literature:: With acetic acid; for 3h; Heating;

Reference yield:

: 22169-71-7
(R)-1-((3aR,5S,6S,6aR)-6-azido-2,2-dimethyltetrahydrofuro-[2,3-d][1,3]dioxol-5-yl)ethane-1,2-diol

: 115996-13-9,116050-86-3
1-((3aR,6aR)-2-Hydroxy-hexahydro-furo[3,2-b]pyrrol-4-yl)-ethanone

Guidance literature:: Multi-step reaction with 8 steps

1: 72 percent / pyridine / Ambient temperature

2: H₂ / 10percent Pd-C / methanol / 10 h / 760 Torr / Ambient temperature

3: NaOAc / ethanol / 4 h / Heating

4: methanol / 2 h / Ambient temperature

5: 76 percent / Amberlite IR 120 (H+) / 6 h / Heating

7: 82 percent / tri-n-butyltin hydride, α,α'-azobisisobutyronitrile / toluene / 8 h / Heating

8: 86 percent / 50percent aq.HOAc / 3 h / Heating

With pyridine; Amberlite IR 120 (H+); azobisisobutyronitrile; hydrogen; tri-n-butyl-tin hydride; sodium acetate; acetic acid; palladium on activated charcoal; In methanol; ethanol; toluene;

Reference yield:

: 107690-58-4
3-azido-3,5-dideoxy-1,2-O-isopropylidene-α-D-xylo-hexofuranose

: 115996-13-9,116050-86-3
1-((3aR,6aR)-2-Hydroxy-hexahydro-furo[3,2-b]pyrrol-4-yl)-ethanone

Guidance literature:: Multi-step reaction with 8 steps

1: 95 percent / pyridine / 1.5 h / Ambient temperature

2: 90 percent / H₂ / 10percent Pd-C / methanol / 18 h / 760 Torr / Ambient temperature

3: 85 percent / NaOAc / ethanol / 6 h / Heating

4: 81 percent / pyridine / 2 h / Ambient temperature

5: 85 percent / Amberlite IR 120 (H+) / 3 h / Heating

7: 82 percent / tri-n-butyltin hydride, α,α'-azobisisobutyronitrile / toluene / 8 h / Heating

8: 86 percent / 50percent aq.HOAc / 3 h / Heating

With pyridine; Amberlite IR 120 (H+); azobisisobutyronitrile; hydrogen; tri-n-butyl-tin hydride; sodium acetate; acetic acid; palladium on activated charcoal; In methanol; ethanol; toluene;