iodo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane

Base Information

• Chemical Name: iodo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane
• CAS No.: 201471-46-7
• Molecular Formula: C₂₅H₄₇INPSi₂
• Molecular Weight: 575.704

Synonyms:iodo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane

Chemical Property of iodo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane

Chemical Property:

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Technology Process of iodo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane

There total 1 articles about iodo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

C28H56NPSi3 (188254-66-2) → iodo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane (201471-46-7)

Guidance literature:

With iodine; In tetrahydrofuran; at -40 - 20 ℃;

DOI:10.1002/(SICI)1099-0682(199801)1998:1<83::AID-EJIC83>3.0.CO;2-K

Reference yield: 86.7%

iodo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane (201471-46-7) → chloro[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane

Guidance literature:

With silver(I) chloride; In dichloromethane; for 12h; Ambient temperature;

DOI:10.1002/(SICI)1099-0682(199801)1998:1<83::AID-EJIC83>3.0.CO;2-K

Reference yield:

iodo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane (201471-46-7) → bromo[(2,4,6-tri-tert-butylphenyl)imino](bis(trimethylsilyl)methylene)phosphorane

Guidance literature:

Multi-step reaction with 2 steps

1: 86.7 percent / AgCl / CH₂Cl₂ / 12 h / Ambient temperature

2: 87.5 percent / Me₃SiBr / tetrahydrofuran / 2 h / Ambient temperature

With trimethylsilyl bromide; silver(I) chloride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/(SICI)1099-0682(199801)1998:1<83::AID-EJIC83>3.0.CO;2-K

upstream raw materials:

C₂₈H₅₆NPSi₃

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