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Technology Process of (SiS,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole

(SiS,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole

Base Information
  • Chemical Name:(SiS,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole
  • CAS No.:1126532-55-5
  • Molecular Formula:C25H31NO2Si
  • Molecular Weight:405.612
  • Hs Code.:
(<sup>Si</sup>S,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole

Synonyms:(SiS,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole

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Chemical Property of (SiS,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole
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Technology Process of (SiS,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole

There total 1 articles about (SiS,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

(<sup>Si</sup>R)-1-tert-butyl-1-silaindane
1028869-67-1

(SiR)-1-tert-butyl-1-silaindane

rac-2-(4,5-dimethyloxazol-2-yl)-1-phenylethan-2-ol
76346-89-9

rac-2-(4,5-dimethyloxazol-2-yl)-1-phenylethan-2-ol

C<sub>13</sub>H<sub>15</sub>NO<sub>2</sub>
1126532-74-8

C13H15NO2

(<sup>Si</sup>S,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole
1126532-55-5

(SiS,S)-2-[2-(1-tert-butyl-1-silaindanyl-1-oxy)-2-phenylethyl]-4,5-dimethyloxazole

Guidance literature:
With tris(3,5-dimethylphenyl)phosphine; copper(l) chloride; sodium t-butanolate; In toluene; at 20 ℃; for 2h; optical yield given as %ee; stereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.200801377
upstream raw materials:

(SiR)-1-tert-butyl-1-silaindane

rac-2-(4,5-dimethyloxazol-2-yl)-1-phenylethan-2-ol

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