C₄₅H₅₄N₂O₁₉S₂

Base Information

Chemical Name:C₄₅H₅₄N₂O₁₉S₂
CAS No.:1383527-18-1
Molecular Formula:C₄₅H₅₄N₂O₁₉S₂
Molecular Weight:991.058
Hs Code.:

C<sub>45</sub>H<sub>54</sub>N<sub>2</sub>O<sub>19</sub>S<sub>2</sub>

Synonyms:C₄₅H₅₄N₂O₁₉S₂

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Chemical Property of C₄₅H₅₄N₂O₁₉S₂

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Technology Process of C₄₅H₅₄N₂O₁₉S₂

There total 4 articles about C₄₅H₅₄N₂O₁₉S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383446-50-1
C₅₉H₆₈N₄O₁₂Si

: 1383527-18-1
C₄₅H₅₄N₂O₁₉S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine / 48 h / 20 °C

2.1: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 10 h / 55 °C

2.2: solid phase reaction

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 48 h / 20 °C

4.1: pyridine / 48 h / 20 °C

5.1: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 10 h / 55 °C

5.2: solid phase reaction

6.1: magnesium bromide diethyl etherate / diethyl ether; nitromethane / 48 h / 20 °C

With magnesium bromide diethyl etherate; tetrabutyl ammonium fluoride; sulfur trioxide trimethylamine complex; In tetrahydrofuran; pyridine; diethyl ether; nitromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.04.010

Reference yield:

: 2C₆H₁₅N*C₆₁H₇₂N₂O₁₉S₂Si

: 1383527-18-1
C₄₅H₅₄N₂O₁₉S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 48 h / 20 °C

2.1: pyridine / 48 h / 20 °C

3.1: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 10 h / 55 °C

3.2: solid phase reaction

4.1: magnesium bromide diethyl etherate / diethyl ether; nitromethane / 48 h / 20 °C

With magnesium bromide diethyl etherate; tetrabutyl ammonium fluoride; sulfur trioxide trimethylamine complex; In tetrahydrofuran; pyridine; diethyl ether; nitromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.04.010

Reference yield:

: 1383446-43-2
C₅₁H₆₈N₂O₁₄Si

: 1383527-18-1
C₄₅H₅₄N₂O₁₉S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 10 h / 55 °C

1.2: solid phase reaction

2.1: magnesium bromide diethyl etherate / diethyl ether; nitromethane / 48 h / 20 °C

With magnesium bromide diethyl etherate; sulfur trioxide trimethylamine complex; In diethyl ether; nitromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.04.010