4-bromo-N-mesitylsydnone

Base Information

• Chemical Name: 4-bromo-N-mesitylsydnone
• CAS No.: 104412-10-4
• Molecular Formula: C₁₁H₁₁BrN₂O₂
• Molecular Weight: 283.125
• Mol file: 104412-10-4.mol

Synonyms:4-bromo-N-mesitylsydnone

Chemical Property of 4-bromo-N-mesitylsydnone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-bromo-N-mesitylsydnone

There total 1 articles about 4-bromo-N-mesitylsydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3‐(2,4,6-trimethylphenyl)sydnone (104411-99-6) → 4-bromo-N-mesitylsydnone (104412-10-4)

Guidance literature:

With bromine; sodium hydrogencarbonate; In ethanol; water; for 0.5h;

Reference yield: 95.0%

carbon dioxide (124-38-9,18923-20-1) + 4-bromo-N-mesitylsydnone (104412-10-4) → lithium N-mesitylsydnone-4-carboxylate

Guidance literature:

4-bromo-N-mesitylsydnone; With n-butyllithium; In diethyl ether; cyclohexane; at -50 ℃; for 0.5h; Inert atmosphere;

carbon dioxide; In diethyl ether; cyclohexane; at -50 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2018.03.019

Reference yield: 80.0%

4-bromo-N-mesitylsydnone (104412-10-4) → 3‐(2,4,6-trimethylphenyl)sydnone (104411-99-6)

Guidance literature:

With sodium sulfite; In methanol; water;

upstream raw materials:

3‐(2,4,6-trimethylphenyl)sydnone

Downstream raw materials:

3‐(2,4,6-trimethylphenyl)sydnone