H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)

Base Information

Chemical Name:H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)
CAS No.:146128-78-1
Molecular Formula:C₂₁H₃₃AlAsN
Molecular Weight:401.403
Hs Code.:

H<sub>2</sub>AlAs(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)2(N(CH<sub>3</sub>)3)

Synonyms:H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)

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Chemical Property of H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)

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Technology Process of H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)

There total 1 articles about H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 6401-80-5
trimethylamine-chloroalane

: 101860-08-6
bis(2,4,6-trimethylphenyl)arsane

: 146128-78-1
H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)

Guidance literature:: With n-butyl lithium; In diethyl ether; treatment of (mesityl)2AsH in Et2O with n-BuLi at -78°C under stirring; warming to 25°C and stirring for 1 h; the -78°C cooled soln. was added dropwise to a soln. of H2AlCl*NMe3 in Et2O at -78°C;; removal of solvent and volatiles under reduced pressure; the residue was extracted with toluene; filtration; crystn. from filtrate after concn.; recrystn. from toluene; elem. anal.;;
DOI:10.1021/om00025a008