H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)

Base Information

• Chemical Name: H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)
• CAS No.: 146128-78-1
• Molecular Formula: C₂₁H₃₃AlAsN
• Molecular Weight: 401.403
• Mol file: 146128-78-1.mol

Synonyms:H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)

Chemical Property of H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)

Chemical Property:

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Technology Process of H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3)

There total 1 articles about H₂AlAs(C₆H₂(CH₃)3)2(N(CH₃)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

trimethylamine-chloroalane (6401-80-5) + bis(2,4,6-trimethylphenyl)arsane (101860-08-6) → H2AlAs(C6H2(CH3)3)2(N(CH3)3) (146128-78-1)

Guidance literature:

With n-butyl lithium; In diethyl ether; treatment of (mesityl)2AsH in Et2O with n-BuLi at -78°C under stirring; warming to 25°C and stirring for 1 h; the -78°C cooled soln. was added dropwise to a soln. of H2AlCl*NMe3 in Et2O at -78°C;; removal of solvent and volatiles under reduced pressure; the residue was extracted with toluene; filtration; crystn. from filtrate after concn.; recrystn. from toluene; elem. anal.;;

DOI:10.1021/om00025a008

upstream raw materials:

trimethylamine-chloroalane

bis(2,4,6-trimethylphenyl)arsane