4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2β-hydroxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one

Base Information

Chemical Name:4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2β-hydroxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one
CAS No.:182236-70-0
Molecular Formula:C₂₆H₄₀O₅Si
Molecular Weight:460.686
Hs Code.:

Synonyms:4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2β-hydroxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one

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Chemical Property of 4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2β-hydroxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one

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Technology Process of 4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2β-hydroxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one

There total 2 articles about 4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2β-hydroxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 17697-12-0
benzeneseleninic anhydride

: 182236-67-5
4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one

: 182236-70-0
4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2β-hydroxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one

: C₂₆H₄₀O₄Si

: C₃₂H₄₄O₅SeSi

Guidance literature:: With potassium tert-butylate; triethyl phosphite; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(96)01495-5 DOI:10.1016/S0040-4020(98)00056-8

Reference yield: 72.0%

: 182236-67-5
4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one

: 182236-70-0
4β,11β-dihydro-7β-(tert-butyldimethylsilyl)oxy-2β-hydroxy-2α,20α-oxido-20-oxo-taxane-3,12-diene-10-one

: C₂₆H₄₀O₄Si

: C₃₂H₄₄O₅SeSi

Guidance literature:: With (PhSeO)2O; potassium tert-butylate; triethyl phosphite; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(96)01495-5