({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide

Base Information

Chemical Name:({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide
CAS No.:1345418-12-3
Molecular Formula:C₃₂H₃₆N₈O₅
Molecular Weight:612.688
Hs Code.:

({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide

Synonyms:({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide

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Chemical Property of ({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide

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Technology Process of ({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide

There total 5 articles about ({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345418-07-6
[(E)-(3-methoxyphenyl)diazenyl]benzoic acid

: 478804-08-9
4-amino-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}-carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide

: 1345418-12-3
({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide

Guidance literature:: With 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.08.035

Reference yield:

: 619-50-1
4-nitrobenzoic acid methyl ester

: 1345418-12-3
({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 24 h / Inert atmosphere; Reflux

2.1: lithium hydroxide / methanol; water / 24 h / 70 °C

2.2: pH 6

3.1: 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide

With 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; lithium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.08.035

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 1345418-12-3
({4-[(E)-(3-methoxyphenyl)diazenyl]benzoyl}amino)-1-methyl-N-[1-methyl-5-({[2-(4-morpholinyl)ethyl]amino}carbonyl)-1H-pyrrol-3-yl]-1H-pyrrole-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 24 h / Inert atmosphere; Reflux

2.1: lithium hydroxide / methanol; water / 24 h / 70 °C

2.2: pH 6

3.1: 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide

With 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; lithium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.08.035