(R)-2,6,7,8-tetrahydro-N-methyl-6-methylene-2-tosyl-N-(2-vinylbut-3-enyl)benzo[cd]indol-7-amine

Base Information

Chemical Name:(R)-2,6,7,8-tetrahydro-N-methyl-6-methylene-2-tosyl-N-(2-vinylbut-3-enyl)benzo[cd]indol-7-amine
CAS No.:1228274-04-1
Molecular Formula:C₂₆H₂₈N₂O₂S
Molecular Weight:432.587
Hs Code.:

Synonyms:(R)-2,6,7,8-tetrahydro-N-methyl-6-methylene-2-tosyl-N-(2-vinylbut-3-enyl)benzo[cd]indol-7-amine

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Chemical Property of (R)-2,6,7,8-tetrahydro-N-methyl-6-methylene-2-tosyl-N-(2-vinylbut-3-enyl)benzo[cd]indol-7-amine

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Technology Process of (R)-2,6,7,8-tetrahydro-N-methyl-6-methylene-2-tosyl-N-(2-vinylbut-3-enyl)benzo[cd]indol-7-amine

There total 1 articles about (R)-2,6,7,8-tetrahydro-N-methyl-6-methylene-2-tosyl-N-(2-vinylbut-3-enyl)benzo[cd]indol-7-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-93-5
1,4-Pentadiene

: C₂₂H₂₄N₂O₃S

: 1228274-04-1
(R)-2,6,7,8-tetrahydro-N-methyl-6-methylene-2-tosyl-N-(2-vinylbut-3-enyl)benzo[cd]indol-7-amine

: C₂₆H₂₈N₂O₂S

Guidance literature:: 1,4-Pentadiene; With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

With zinc dibromide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

C₂₂H₂₄N₂O₃S; In tetrahydrofuran; at -78 - 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol100819f

Reference yield: 54.0%

: 1228274-04-1
(R)-2,6,7,8-tetrahydro-N-methyl-6-methylene-2-tosyl-N-(2-vinylbut-3-enyl)benzo[cd]indol-7-amine

: 1228274-09-6
(6aR,9S)-7-methyl-4-tosyl-9-vinyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinoline

: 1228274-03-0
(6aR,9R)-7-methyl-4-tosyl-9-vinyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinoline

Guidance literature:: With (2,6-diisopropylphenylimide){3,3′-di(t-butyl)-5,5′,6,6′-tetramethyl-2,2′-biphenoxy}neophylidenemolybdenum(VI); In benzene; for 0.5h; diastereoselective reaction; Microwave irradiation;
DOI:10.1021/ol100819f